| Injection |
1.0 µL. Injector Temperature 325ºC. Pressure 70.1 kPa. Split: 10:1. |
| First column |
30 m X 0.25 mm X 0.50 µm, 50% Phenyl Polysilphenylene siloxane (BPX50, SGE Analytical Sc. Austin, TX). |
| Modulator |
Period 4.0 s. Con1 330ºC |
| Second column |
2 m X 0.1 mm X 0.1 µm, 100% Polydimethylsiloxane (BPX1, SGE Analytical Sc., Austin, TX). |
| Oven program |
40ºC for 2 min. 40-325ºC @ 5ºC min-1 Hold at 325 ºC for 30 min. |
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