Drawout
plate
(mm)

aSource
(ºC)

Scan
tr
(min)

Scan
% m/z
111/112

Scan
% m/z
125/112

Scan
% m/z
182/112

SIM
tr
(min)

SIM
% m/z
111/112

SIM
% m/z
125/112

 

 

 

 

 

 

 

 

 

3

230

15.17

22

15

3

15.18

23

15

 

250

15.17

23

15

3

15.18

23

15

 

270

15.18

23

15

2

15.18

24

15

 

290

15.18

24

16

2

15.18

26

16

 

310

15.17

25

15

1

15.18

26

16

 

330

15.18

28

15

1

15.18

27

16

 

350

15.18

26

17

1

15.18

28

16

Mean

 

15.18

25

15

2

15.18

25

16

SD

 

0.00

2

1

1

0.00

2

1

RSD%

 

0.01

7.58

4.61

41.17

0.00

7.09

4.30

 

 

 

 

 

 

 

 

 

6

230

15.17

22

14

3

15.17

22

15

 

250

15.17

24

14

2

15.17

24

15

 

270

15.17

24

14

2

15.17

24

15

 

290

15.18

24

15

2

15.18

25

15

 

310

15.17

26

16

1

15.18

26

15

 

330

15.18

27

16

1

15.18

27

16

 

350

15.18

28

16

1

15.18

28

16

Mean

 

15.17

25

15

2

15.18

25

15

SD

 

0.01

2

1

1

0.01

2

1

RSD%

 

0.04

7.75

5.81

36.40

0.04

7.13

3.63

atemperature
Table 6: Scan and SIM mode mass spectral analysis of GSM by liquid auto sampler injection.