| |
XRD |
BET |
Granulometer |
| Sample
(0.8 mm balls) |
Slope (1/ε) |
Diameter (ε) μm |
BET surface area (m2/g) |
Diameter (μm) |
Granulometer
average diameter (μm) |
| 5 min |
0.016 |
0.0625 |
8.839 |
0.17 |
0.57 |
| 10 min |
0.014 |
0.0714 |
10.666 |
0.14 |
0.36 |
| 20 min |
0.014 |
0.0714 |
13.396 |
0.11 |
* |
| 30 min |
0.016 |
0.0625 |
15.667 |
0.10 |
* |
| 40 min |
0.015 |
0.0666 |
17.671 |
0.09 |
* |
| Sample
(0.4 mm balls) |
Slope (1/ε) |
Diameter (ε) μm |
BET surface area (m2/g) |
Diameter (μm) |
Granulometer
average diameter(μm) |
| 5 min |
0.0127 |
0.0786 |
8.3650 |
0.18 |
0.20 |
| 10 min |
0.0151 |
0.0662 |
10.234 |
0.15 |
0.10 |
| 20 min |
0.0154 |
0.0649 |
12.446 |
0.12 |
0.15 |
| 30 min |
0.0211 |
0.0473 |
16.254 |
0.09 |
0.14 |
| 40 min |
0.0194 |
0.0515 |
15.849 |
0.10 |
0.08 |
*The average Granulometric diameter for the 20, 30 and 40 min samples was not mentioned because aggregates were formed at 20 min and hence, the granulometric
results would not be longer valid |
