1 In Burette Nitrite solution
2 In conical flask 10 cm3 0.1 N KMnO4+90 cm3 1 N H2SO4+ potato pieces ( 0.5 g for NaNO2 and 2.00 g for KNO2
3 Indicator KMnO4 itself
4 End point Pink to colourless
Table 4a: Three burette readings were recorded and CBR was recorded as X cm3 for nitrite solution.