| Material |
Composition |
Mode of Application |
| Clearfil SE Bond (CSEB) (Kuraray Co. Ltd., Osaka, Japan)
Two step SE adhesive
(water-based) |
1- primer: 10-MDP, HEMA, hydrophilic DMA,dicamphorquinone, N,N-diethanol-p-touidine; water. |
Apply primer for 20 s, Mild air stream |
| 2- Bond: 10-MDP, Bis-GMA, HEMA, hydrophilic DMA,Dicamphorquinone, N,N-diethanol-p-touidine, silanated colloidal silica. pH 1.4- 2 dry bonding
lot n: 51435 |
Apply bond, Gentle air stream |
| Light cure for 10 s. |
| Apply composite. |
| Clearfil S³ Bond (CSB)(Kuraray Medical Inc.,Okayama, Japan)one step SE adhesive (water and ethanol-based)
|
10-MDP, HEMA, Bis-GMA, water, ethanol,silanated colloidal silica, camphorquinone.pH 2.7- dry bonding
lot n 00143A
|
Apply for 20 seconds |
| Dry with air pressure for 5 seconds |
| Light cure for 10 seconds. |
| Apply composite. |
| IBond (HaraeusKulzer,Armonk,Inc.NY USA)
|
UDMA, 4-META, glutaraldehyde, water, acetone,photoinitiators, stabilizers; pH 2.1; Batch: 010084 dry bonding
|
Shake the bottle; |
| dry; apply 1 layer onto surface cavity; |
| agitate slightly for 20 s; |
| evaporate solvent by air flow for 5-10 s |
| Apply multiple times if cavity does not appear shiny |
| Lightcure for 20 s |
| Apply (water and acetone-based)5-10 s; one step SE adhesive surface composite. |
| Adper Single Bond2 (3M-ESPE, Saint Paul,USA) cavity surface composite.
|
Etchant: 35% H3PO4; colloidal silica pH 0.6 |
Etch for 15 s; rinse for 10 s |
| Adhesive: DMA, HEMA, polyalkenoid acid copolymer, 5 nm silane treated colloidal silica, water, ethanol,photoinitiator; pH 4.3-4.7 - wet; Batch: 4BC bonding lot n N353034
|
blot excess water with a cotton pellet |
| Etch and rinse two-step adhesive system as a control (glistening surface without pooling of water); |
| apply 2 consecutive coats of adhesive by micro- brushing gently on the cavity surface; |
| evaporate solvent by gentle air stream for 5 s; |
| light-cure for 10 s. Apply composite. |
| Filtek Z250 Micro-hybrid resin Composite (3M ESPE, St. paul, MN, USA) |
BIS-GMA and Low-viscosity resin of TEGDMA, a blend of UDMA and Bis-EMA, filled to 60% by volume with zirconia/silica particles a size range of 0.01 to 3.5 microns and an average size of 0.6 micron |
Application of composite in a layers less than 2 mm in thickness and cure with light cure unit for 20s according to Manufacturer’s instructions. |
| BIS-GMA (Bisphenol A glycidaldimethacrylate), TEGDMA (Tri ethylene glycol dimethacrylate), UDMA (urethane dimethacrylate), Bis-EMA: (Bisphenol A polyethylene glycol dietherdimethacrylate), DMA:dimethacrylate, MMA: methyl methacrylate, 4-META: 4-methacryloxy ethyl trimellitateanhydryed, HEMA: 2-hydroxyethyl methacrylate, MDP: 10-methacryloyloxydecyl dihydrogen phosphate, 4-MET: 4-methacryloxy ethyl trimellitic acid; GPDM: glycerol phosphate dimethacrylate; PENTA:dipentaerythritolpentaacrylate phosphate. |
