DPa |
Source b
(°C) |
Scan
tr
(min) |
Scan
% m/z
107/95 |
Scan
% m/z
108/95 |
Scan
% m/z
150/95 |
Scan
% m/z
168/95 |
SIM
tr
(min) |
SIM
% m/z
107/95 |
SIM
% m/z
108/95 |
|
|
|
|
|
|
|
|
|
|
3 mm |
230 |
11.96 |
96 |
34 |
22 |
1.9 |
11.96 |
94 |
35 |
|
250 |
11.96 |
87 |
33 |
19 |
1.7 |
11.96 |
78 |
35 |
|
270 |
11.96 |
82 |
32 |
17 |
1.5 |
11.96 |
85 |
34 |
|
290 |
11.96 |
83 |
32 |
15 |
1.0 |
11.96 |
80 |
33 |
|
310 |
11.96 |
75 |
31 |
13 |
0.8 |
11.96 |
77 |
32 |
|
330 |
11.96 |
77 |
30 |
12 |
0.6 |
11.96 |
78 |
31 |
|
350 |
11.96 |
83 |
27 |
5 |
0.5 |
11.96 |
82 |
30 |
Mean |
|
|
83 |
31 |
15 |
1.1 |
|
82 |
33 |
SD |
|
|
7 |
2 |
5 |
0.5 |
|
6 |
2 |
RSD% |
|
|
8.47 |
7.56 |
37.00 |
47.54 |
|
7.11 |
6.00 |
|
|
|
|
|
|
|
|
|
|
6 mm |
230 |
11.96 |
31 |
23 |
23 |
2.1 |
11.96 |
36 |
27 |
|
250 |
11.96 |
33 |
24 |
22 |
1.4 |
11.96 |
35 |
26 |
|
270 |
11.96 |
32 |
24 |
22 |
1.6 |
11.96 |
33 |
26 |
|
290 |
11.96 |
30 |
23 |
17 |
1.1 |
11.96 |
31 |
24 |
|
310 |
11.96 |
27 |
22 |
13 |
0.9 |
11.96 |
28 |
23 |
|
330 |
11.96 |
26 |
22 |
13 |
0.8 |
11.96 |
28 |
22 |
|
350 |
11.96 |
26 |
21 |
7 |
0.7 |
11.96 |
28 |
21 |
Mean |
|
|
30 |
23 |
17 |
1.2 |
|
31 |
24 |
SD |
|
|
3 |
1 |
6 |
0.5 |
|
3 |
2 |
RSD% |
|
|
9.84 |
4.42 |
36.17 |
38.95 |
|
11.18 |
8.83 |
a Drawout plate
btemperature |
