Drawout
plate |
Source temperature |
tr
(min) |
% m/z
95/107 |
% m/z
108/107 |
aArea
12/9 min |
tr
(min) |
2-MIB
% m/z
107/95 |
2-MIB
% m/z
108/95 |
|
|
|
|
|
|
|
|
|
3 mm |
230 |
9.16 |
35 |
22 |
1.4 |
11.99 |
62 |
43 |
|
250 |
9.17 |
35 |
21 |
2.0 |
11.99 |
68 |
43 |
|
270 |
9.18 |
34 |
21 |
2.0 |
11.99 |
55 |
40 |
|
290 |
9.18 |
34 |
21 |
1.7 |
11.99 |
73 |
35 |
|
310 |
9.18 |
34 |
20 |
1.8 |
12.00 |
55 |
29 |
|
330 |
9.18 |
31 |
20 |
2.4 |
12.00 |
65 |
33 |
|
350 |
9.18 |
31 |
20 |
2.7 |
11.99 |
68 |
31 |
Mean |
|
9.18 |
33 |
21 |
2.0 |
11.99 |
64 |
36 |
SD |
|
0.01 |
2 |
1 |
0.4 |
0.01 |
7 |
6 |
RSD% |
|
0.09 |
5.14 |
3.65 |
21.79 |
0.04 |
10.71 |
15.81 |
|
|
|
|
|
|
|
|
|
6 mm |
230 |
9.19 |
21 |
14 |
2.2 |
12 |
64 |
20 |
|
250 |
9.19 |
23 |
15 |
3.1 |
12 |
54 |
30 |
|
270 |
9.18 |
33 |
19 |
3.7 |
11.99 |
46 |
31 |
|
290 |
9.18 |
33 |
21 |
3.4 |
11.99 |
44 |
28 |
|
310 |
9.19 |
35 |
21 |
3.8 |
11.99 |
41 |
25 |
|
330 |
9.19 |
26 |
15 |
3.2 |
12 |
40 |
25 |
|
350 |
9.19 |
30 |
20 |
3.9 |
12 |
39 |
16 |
Mean |
|
9.19 |
29 |
18 |
3.3 |
12.00 |
47 |
25 |
SD |
|
0.01 |
5 |
3 |
0.6 |
0.01 |
9 |
5 |
RSD% |
|
0.05 |
18.94 |
17.24 |
17.49 |
0.05 |
19.42 |
21.66 |
aRatio of : Area of peak at ± 12.0 min /area of peak at ± 9.2 min |
