| |
Measured concentration |
CV (%) |
RE (%) |
| Spiked |
Intraday (n=6) |
Interday (n=5) |
Intraday (n=6) |
Interday (n=5) |
Intraday (n=6) |
Interday (n=5) |
| 0.25 |
0.28 ± 0.01 |
0.24 ± 0.02 |
4.36 |
8.78 |
11.55 |
-4.13 |
| 0.5 |
- |
0.51 ± 0.02 |
- |
4.52 |
- |
1.42 |
| 1 |
- |
1.01 ± 0.04 |
- |
4.16 |
- |
1.33 |
| 2 |
1.98 ± 0.02 |
1.98 ± 0.04 |
1.03 |
1.96 |
-0.85 |
-0.87 |
| 4 |
3.94 ± 0.03 |
3.94 ± 0.07 |
0.74 |
1.67 |
-1.57 |
-1.56 |
| 8 |
7.94 ± 0.03 |
8.10 ± 0.07 |
0.33 |
0.87 |
-0.79 |
1.22 |
| 12 |
11.81 ± 0.05 |
12.03 ± 0.14 |
0.47 |
1.18 |
-1.60 |
0.28 |
| 15 |
- |
14.94 ± 0.13 |
- |
0.88 |
- |
-0.40 |
All concentrations in nmol*mL-1; CV, coefficient of variation; RE, relative error [(measured concentration−spiked concentration)/spiked concentration×100]. |
