| |
Controla |
Citron oil +Citralb |
Hexanal+ 2-(E)-hexenalc |
Citrald |
Citral +Hexanale |
Hexanalf |
Citral + 2-(E)-hexenalg |
Citron oil+ Carvacrolh |
| Compounds |
T0 |
T3 |
T10 |
T0 |
T3 |
T10 |
T0 |
T3 |
T10 |
T0 |
T3 |
T10 |
T0 |
T3 |
T10 |
T0 |
T3 |
T10 |
T0 |
T3 |
T10 |
T0 |
T3 |
T10 |
| Ethyl acetate |
0.0 |
4.3 |
2.5 |
2.5 |
7.5 |
3.6 |
0.8 |
12.7 |
34.3 |
6.4 |
13.5 |
14.6 |
1.2 |
10.3 |
11.0 |
1.2 |
19.3 |
33.9 |
0.6 |
15.2 |
14.6 |
3.7 |
23.3 |
38.7 |
| Acetic acid, isobutyl ester |
0.6 |
1.2 |
5.6 |
0.0 |
0.0 |
0.0 |
0.0 |
0.0 |
1.0 |
0.0 |
0.0 |
0.0 |
0.0 |
0.0 |
0.3 |
0.0 |
0.2 |
0.6 |
0.0 |
0.0 |
0.5 |
0.0 |
0.0 |
0.0 |
| Acetic acid, butyl ester |
6.9 |
10.9 |
1.8 |
6.0 |
4.7 |
0.0 |
0.8 |
4.4 |
7.9 |
12.9 |
5.2 |
7.6 |
1.3 |
5.5 |
6.0 |
6.1 |
13.6 |
9.3 |
5.2 |
11.5 |
11.6 |
0.8 |
2.5 |
5.1 |
| 1-butanol, 2-methyl-acetate |
11.0 |
11.5 |
12.3 |
5.6 |
4.0 |
0.0 |
1.1 |
1.4 |
4.8 |
23.7 |
11.8 |
5.2 |
4.3 |
5.5 |
1.7 |
15.3 |
27.5 |
3.6 |
5.9 |
10.0 |
2.8 |
2.6 |
4.1 |
4.3 |
| Acetic acid, hexyl ester |
16.4 |
42.2 |
12.6 |
7.3 |
22.0 |
4.2 |
235.1 |
460.8 |
74.0 |
20.6 |
57.2 |
36.8 |
25.0 |
167.3 |
12.2 |
236.5 |
431.6 |
259.3 |
31.3 |
171.6 |
53.5 |
6.9 |
26.0 |
20.3 |
| 2-Hexen-1-ol, acetate |
0.0 |
0.0 |
0.0 |
0.0 |
0.0 |
0.0 |
46.4 |
9.5 |
0.8 |
0.0 |
0.0 |
0.0 |
0.0 |
0.0 |
0.0 |
0.0 |
0.0 |
0.0 |
13.1 |
3.0 |
0.2 |
0.0 |
0.0 |
0.0 |
| Butanoic acid methyl esters |
0.0 |
0.0 |
0.0 |
0.4 |
1.0 |
0.0 |
0.0 |
0.1 |
0.0 |
3.4 |
6.8 |
3.9 |
5.6 |
3.8 |
0.0 |
5.2 |
11.1 |
0.0 |
0.7 |
7.9 |
1.1 |
0.0 |
0.0 |
0.0 |
| Citronellyl acetate |
0.0 |
0.0 |
0.0 |
0.3 |
5.4 |
1.9 |
0.0 |
0.0 |
0.0 |
1.4 |
9.5 |
11.1 |
1.5 |
10.2 |
0.4 |
0.0 |
0.0 |
0.0 |
1.2 |
21.8 |
4.0 |
0.0 |
0.0 |
0.0 |
| Linalyl butyrate |
0.0 |
0.0 |
0.0 |
4.9 |
5.4 |
0.3 |
0.0 |
0.0 |
0.0 |
0.0 |
0.0 |
0.0 |
0.0 |
0.0 |
0.0 |
0.0 |
0.0 |
0.0 |
0.0 |
0.0 |
0.0 |
28.4 |
26.6 |
8.3 |
| Total Esters |
34.9 |
70.0 |
34.7 |
26.9 |
50.0 |
10.1 |
284.2 |
489.0 |
122.8 |
68.5 |
104.1 |
79.2 |
38.9 |
202.6 |
31.6 |
264.3 |
503.3 |
306.6 |
58.0 |
240.9 |
88.2 |
42.4 |
82.5 |
76.6 |
| Hexane |
0.0 |
0.0 |
0.0 |
0.0 |
0.0 |
0.0 |
0.0 |
0.0 |
0.0 |
0.0 |
0.0 |
7.5 |
0.0 |
0.0 |
0.0 |
0.0 |
0.3 |
0.0 |
6.4 |
0.0 |
0.0 |
0.0 |
0.0 |
0.0 |
| β-myrcene |
0.0 |
0.0 |
0.0 |
0.4 |
0.3 |
0.0 |
0.0 |
0.0 |
0.0 |
0.0 |
0.0 |
0.0 |
0.0 |
0.0 |
0.0 |
0.0 |
0.0 |
0.0 |
0.0 |
0.0 |
0.0 |
4.1 |
3.6 |
2.0 |
| Limonene |
0.4 |
1.7 |
1.4 |
38.6 |
28.3 |
2.6 |
0.0 |
0.4 |
0.9 |
1.0 |
1.3 |
0.9 |
1.7 |
0.5 |
0.0 |
0.7 |
0.2 |
0.0 |
0.5 |
1.1 |
0.3 |
213.0 |
203.1 |
124.8 |
| α Terpinene |
0.0 |
0.0 |
0.0 |
19.7 |
19.0 |
1.5 |
0.0 |
0.0 |
0.0 |
0.0 |
0.0 |
0.0 |
0.0 |
0.0 |
0.0 |
0.0 |
0.0 |
0.0 |
0.0 |
0.0 |
0.0 |
155.5 |
126.9 |
72.1 |
| Cymene |
0.0 |
0.0 |
0.0 |
13.3 |
3.1 |
0.0 |
0.0 |
0.0 |
0.0 |
0.0 |
0.0 |
0.0 |
0.0 |
0.0 |
0.0 |
0.0 |
0.0 |
0.0 |
0.0 |
0.0 |
0.0 |
35.0 |
66.3 |
55.2 |
| β-pinene |
0.0 |
0.0 |
0.0 |
3.1 |
1.6 |
0.0 |
0.0 |
0.0 |
0.0 |
0.0 |
0.0 |
0.0 |
0.0 |
0.0 |
0.0 |
0.0 |
0.0 |
0.0 |
0.0 |
0.0 |
0.0 |
8.7 |
8.0 |
4.4 |
| thymol methyl ether |
0.0 |
0.0 |
0.0 |
0.0 |
0.0 |
0.0 |
0.0 |
0.0 |
0.0 |
0.0 |
0.0 |
0.0 |
0.0 |
0.0 |
0.0 |
0.0 |
0.0 |
0.0 |
0.0 |
0.0 |
0.0 |
0.0 |
18.0 |
11.0 |
| Total Hydrocarbons |
0.4 |
1.7 |
1.4 |
75.0 |
52.2 |
4.0 |
0.0 |
0.4 |
0.9 |
1.0 |
1.3 |
8.4 |
1.7 |
0.5 |
0.0 |
0.7 |
0.5 |
0.0 |
6.9 |
1.1 |
0.3 |
416.4 |
426.0 |
269.4 |
| Nerol |
0.0 |
0.0 |
0.0 |
1.9 |
0.0 |
0.0 |
0.0 |
0.0 |
0.0 |
4.3 |
0.0 |
0.0 |
1.8 |
0.0 |
0.0 |
0.0 |
0.0 |
0.0 |
2.6 |
0.0 |
0.0 |
0.0 |
0.0 |
0.0 |
| Geraniol |
0.0 |
0.0 |
0.0 |
1.8 |
0.0 |
0.0 |
0.0 |
0.0 |
0.0 |
5.0 |
0.0 |
0.0 |
1.4 |
0.0 |
0.0 |
0.0 |
0.0 |
0.0 |
2.2 |
0.0 |
0.0 |
0.0 |
0.0 |
0.0 |
| Carvacrol |
0.0 |
0.0 |
0.0 |
0.0 |
0.0 |
0.0 |
0.0 |
0.0 |
0.0 |
0.0 |
0.0 |
0.0 |
0.0 |
0.0 |
0.0 |
0.0 |
0.0 |
0.0 |
0.0 |
0.0 |
0.0 |
27.4 |
15.5 |
0.0 |
| β-citronellol |
0.0 |
0.0 |
0.0 |
39.6 |
58.3 |
33.4 |
0.0 |
0.0 |
0.0 |
63.7 |
144.3 |
81.1 |
44.8 |
64.8 |
4.7 |
0.0 |
0.0 |
0.0 |
42.4 |
72.1 |
21.5 |
6.5 |
6.0 |
0.0 |
| Hexanol |
2.5 |
1.7 |
0.0 |
8.4 |
3.0 |
3.8 |
33.1 |
8.4 |
2.6 |
9.5 |
11.0 |
11.4 |
33.3 |
17.8 |
2.6 |
35.2 |
10.2 |
7.6 |
21.0 |
16.3 |
5.6 |
1.5 |
2.4 |
1.5 |
| Ethanol |
0.6 |
0.9 |
0.0 |
12.0 |
10.8 |
6.1 |
11.0 |
8.9 |
8.0 |
14.0 |
12.2 |
10.3 |
11.5 |
10.3 |
4.9 |
14.1 |
12.0 |
8.7 |
10.8 |
11.5 |
7.4 |
14.5 |
14.1 |
9.3 |
| Total Alcohols |
3.1 |
2.6 |
0.0 |
63.7 |
72.0 |
43.3 |
44.1 |
17.2 |
10.6 |
96.5 |
167.5 |
102.9 |
92.8 |
92.9 |
12.2 |
49.3 |
22.2 |
16.3 |
79.0 |
99.9 |
34.5 |
49.9 |
38.0 |
10.8 |
| Hexanal |
24.6 |
35.6 |
24.0 |
18.2 |
55.5 |
38.5 |
3.9 |
2.7 |
16.5 |
9.9 |
27.7 |
20.0 |
31.5 |
26.1 |
28.8 |
14.7 |
11.3 |
10.4 |
16.3 |
20.2 |
30.2 |
5.1 |
6.3 |
12.5 |
| Neral |
0.0 |
0.0 |
0.0 |
2.9 |
0.0 |
0.0 |
0.0 |
0.0 |
0.0 |
48.7 |
1.0 |
0.0 |
2.0 |
0.0 |
0.0 |
0.0 |
0.0 |
0.0 |
8.1 |
0.0 |
0.0 |
0.0 |
0.0 |
0.0 |
| Geranial |
0.0 |
0.0 |
0.0 |
3.7 |
0.5 |
0.0 |
0.0 |
0.0 |
0.0 |
48.4 |
1.9 |
0.0 |
3.3 |
0.0 |
0.0 |
0.0 |
0.0 |
0.0 |
8.2 |
0.0 |
0.0 |
0.0 |
0.0 |
0.0 |
| 2-(E)-hexenal |
14.6 |
28.2 |
50.0 |
13.3 |
29.3 |
31.6 |
7.2 |
5.5 |
29.8 |
7.2 |
19.3 |
18.4 |
24.7 |
12.4 |
11.1 |
0.0 |
7.2 |
18.2 |
18.8 |
16.8 |
23.3 |
6.9 |
10.4 |
18.8 |
| Total Aldehydes |
39.2 |
63.7 |
73.9 |
38.0 |
85.3 |
70.0 |
11.1 |
8.2 |
46.3 |
114.1 |
49.9 |
38.4 |
61.5 |
38.5 |
39.9 |
14.7 |
18.5 |
28.5 |
51.4 |
37.0 |
53.5 |
12.0 |
16.7 |
31.2 |
| Total metabolites |
77.5 |
138.1 |
110.1 |
203.6 |
259.6 |
127.4 |
339.3 |
514.8 |
180.6 |
280.1 |
322.9 |
228.9 |
194.9 |
334.5 |
83.6 |
329.0 |
544.6 |
351.4 |
195.3 |
378.9 |
176.5 |
520.6 |
563.1 |
388.1 |
aControl was washed only with dipping solution (1% citric acid + 0.5% ascorbic acid)
bConcentration employed 125 mg L-1 each.
cConcentration employed 125 mg L-1 each.
dConcentration employed 250 mg L-1
eConcentration employed 125 mg L-1 each.
fConcentration employed 250 mg L-1
gConcentration employed 125 mg L-1 each
hConcentration employed 200 mg L-1 citron oil and 50 mg L-1 carvarcol. |
