|
Injector |
Inlet temperature
Sample size
Split ratio |
200˚C
2µl
50 |
|
Column temperature program |
Initial temperature
Rate 1
Rate 2
Rate 3 |
50˚C
15˚C /min to 180˚C
7˚C /min to 230˚C
10˚C /min to 280˚C |
|
Detector |
Type
Interface temperature |
Mass Spectrometer
200˚C |
|
Column |
Type Flow rate |
HP-5MS (30m, 0.25mmID, 0.25µm)
3 mL/min |