| Parameters |
CCC |
RP-HPLC |
Ratio CCC/RP-HPLC |
| Run time/injection (min) |
210 |
60 |
3.5 |
| Mobile phase flow rate (mL min-1) |
2 |
16 |
0.125 |
| Operating pressure (Mpa) |
2 |
19.97 |
0.1 |
| Column volumes (mL) |
300 |
60 |
5 |
| Sample loading/run (mg) |
100 |
100 |
1 |
| Injection volume (mL) |
10 |
2 |
5 |
| Total solvent used |
420 |
960 |
0.437 |
| Purity of five compounds |
Over 95% |
Over 95% |
Close 1 |
| Detector |
ELSD |
UV |
- |
|
