| Drugs |
Conc (μg mL−1) |
Intraday precision |
Interday precision |
| % Rec |
% RSD |
% Rec |
% RSD |
| Phase-1 |
| Lef |
0.625 |
99.88 |
0.168 |
99.57 |
0.102 |
| 1.25 |
100.12 |
0.102 |
99.54 |
0.103 |
| 1.875 |
99.85 |
1.15 |
99.9 |
0.85 |
| 2.5 |
100.05 |
1.06 |
100.11 |
1.45 |
| 5 |
99.19 |
1.14 |
99.66 |
0.74 |
| Flur |
0.625 |
100.26 |
0.39 |
100.29 |
0.58 |
| 1.25 |
100.07 |
0.53 |
100.04 |
0.39 |
| 1.875 |
99.04 |
0.087 |
99.98 |
1.02 |
| 2.5 |
100.01 |
0.192 |
99.94 |
0.042 |
| 5 |
99.61 |
0.48 |
100.2 |
1.08 |
| Ibu |
11.25 |
100.41 |
1.12 |
99.97 |
0.166 |
| 22.5 |
100.02 |
1.02 |
98.54 |
0.32 |
| 33.75 |
100.10 |
0.24 |
100.2 |
1.08 |
| 45 |
99.76 |
0.29 |
99.89 |
0.33 |
| 90 |
99.42 |
0.17 |
100.12 |
0.90 |
| Phase-2 |
| Lef |
0.625 |
99.78 |
0.34 |
99.57 |
0.08 |
| 1.25 |
99.88 |
0.06 |
99.54 |
0.27 |
| 1.875 |
100.02 |
0.02 |
100.29 |
0.29 |
| 2.5 |
99.57 |
0.03 |
100.18 |
0.87 |
| 5 |
100.48 |
0.63 |
99.66 |
0.06 |
| Diclo |
1.56 |
99.46 |
1.13 |
100.16 |
0.18 |
| 6.25 |
100.21 |
0.26 |
99.87 |
0.29 |
| 12.5 |
100.5 |
0.15 |
99.98 |
1.17 |
| 25 |
98.78 |
0.66 |
100.2 |
0.68 |
| 50 |
100.1 |
0.63 |
99.85 |
1.27 |
| Mef |
0.78 |
98.78 |
0.28 |
100.1 |
0.015 |
| 3.125 |
100.03 |
0.86 |
100.54 |
0.97 |
| 6.25 |
100.18 |
1.35 |
98.98 |
0.016 |
| 12.5 |
99.78 |
0.37 |
99.48 |
0.99 |
| 25 |
98.48 |
0.14 |
100.2 |
0.43 |
|