Position |
1 |
2 |
3 |
1 |
0.79 m, 1.68 m |
0.89 m, , 1.86 m |
1.25 m, 1.98 m |
2 |
1.41 m, 1.92 m |
1.34 m, 1.94 m |
1.82 dd (13.2, 12.2), 2.54 dd (12.0, 4.8) |
3 |
1.06 m, 2.34 d (12.4) |
4.12 t (W1/2, 2.60) |
- |
5 |
1.32 m |
1.57 m |
1.83 m |
6 |
1.42 m, 1.72 m |
1.42 m, 1.64 m |
1.40 m, 1.63 m |
7 |
1.32 m, 1.70 m |
1.47 m, 1.66 m |
1.45 m, 1.67 m |
9 |
0.94 m |
0.98 m |
0.97 m |
11 |
1.74 m |
1.65 m |
1.68 m |
12 |
1.76 m, 1.95 m |
1.54 m, 1.70 m |
1.51 m, 1.73 m |
13 |
- |
2.02 m |
1.98 m |
14 |
2.24 m, 2.72 d (12.8) |
1.78 m, 2.41 m |
1.76 m, 2.43 m |
15 |
2.08 m, 2.52 m |
1.35 m, 1.82 m |
1.35 m, 1.82 m |
17 |
5.03 s, 5.56 s |
3.91 d (10.6),
4.49 d ( 10.2) |
3.95 d (10.4),
4.50 d ( 10.8) |
18 |
1.26 s |
0.87 s |
0.93 s |
19 |
- |
1.02 s |
1.02 s |
20 |
1.24 s |
1.17 s |
1.10 s |
1′ |
6.15 d (8.5) |
5.05 d (8.2) |
5.06 d (7.8) |
2′ |
3.96 m |
4.04 m |
4.02 m |
3′ |
4.08 m |
4.46 m |
4.45 m |
4′ |
4.33 m |
4.25 m |
4.23 m |
5′ |
4.21 m |
4.63 m |
4.64 m |
6′ |
4.03 dd (4.2, 12.4),
4.41 dd (2.4, 9.2) |
3.61 dd (4.4, 12.2),
4.27 dd (2.5, 10.6) |
3.60 dd (4.4, 12.0),
4.24 dd (2.3, 10.2) |
1′′ |
5.13 d (7.8) |
|
|
2′′ |
4.19 m |
|
|
3′′ |
4.35 m |
|
|
4′′ |
4.23 m |
|
|
5′′ |
3.38 m |
|
|
6′′ |
4.22 dd (3.9, 12.2),
4.62 dd (2.2, 8.0) |
|
|
aassignments made on the basis of COSY, HSQC and HMBC correlations;
bChemical shift values are in δ (ppm);
cCoupling constants are in Hz. |