a) The experimental parameters used for ICP-MS. |
Parameters |
|
Forward Power |
1500 W |
Reflected Power |
1 W |
Carrier Gas |
1.0 L/min |
S/C Temperature |
2ºC |
Nebulizer Pump |
0.1 rps |
Repetition |
3 |
Uptake Speed |
0.30 rps |
Uptake Time |
30 sec |
Stabilization Time |
45 sec |
|
b) The temperature program of GC-MS. |
Rate (ºC/min) |
Temperature (ºC) |
Hold time (min) |
|
70 |
2 |
5 |
120 |
2 |
3 |
190 |
0 |
5 |
210 |
0 |
10 |
260 |
0 |
5 |
290 |
0 |
|
|
Table 2: The experimental parameters for ICP-MS and GC-MS. |