| a) The experimental parameters used for ICP-MS. |
| Parameters |
|
| Forward Power |
1500 W |
| Reflected Power |
1 W |
| Carrier Gas |
1.0 L/min |
| S/C Temperature |
2ºC |
| Nebulizer Pump |
0.1 rps |
| Repetition |
3 |
| Uptake Speed |
0.30 rps |
| Uptake Time |
30 sec |
| Stabilization Time |
45 sec |
|
| b) The temperature program of GC-MS. |
| Rate (ºC/min) |
Temperature (ºC) |
Hold time (min) |
| |
70 |
2 |
| 5 |
120 |
2 |
| 3 |
190 |
0 |
| 5 |
210 |
0 |
| 10 |
260 |
0 |
| 5 |
290 |
0 |
|
| |
| Table 2: The experimental parameters for ICP-MS and GC-MS. |
