MOXIFLOXACIN-ACCURACY

Spike
level

Wt.of sample
taken in mg

Sample
 area

mg/mL
added

mg/mL
found

% Recovery

% Recovery

Average

50%_01

674.46

1159290

0.04996

0.05454

100.1

100.1

100.1

50%_02

672.90

1155954

0.04984

0.05438

100.1

100.0

50%_03

673.11

1158198

0.04986

0.05449

100.2

100.2

70%_01

1018.65

1753515

0.07545

0.08249

100.3

100.3

100.0

70%_02

1018.42

1746671

0.07544

0.08217

99.9

99.9

70%_03

1016.46

1744562

0.07529

0.08207

100.0

100.0

100%_01

1349.09

2292178

0.09993

0.10783

98.9

99.0

98.6

100%_02

1348.20

2281190

0.09987

0.10732

98.5

98.5

100%_03

1347.63

2272375

0.09982

0.10690

98.2

98.2

125%_01

1686.17

2867979

0.1249

0.13492

99.1

99.1

98.9

125%_02

1685.31

2856118

0.12484

0.13436

98.7

98.7

125%_03

1685.91

2866778

0.12488

0.13487

99.0

99.0

150%_01

2015.68

3400552

0.14931

0.15998

98.3

98.3

98.2

150%_02

2023.69

3406155

0.1499

0.16024

98.0

98.0

150%_03

2021.14

3411601

0.14971

0.16050

98.3

98.3

Acceptance criteria:% Average recovery shall be  between 98.0% -102.0%

Table 9: