| MOXIFLOXACIN-ACCURACY |
Spike
level |
Wt.of sample
taken in mg |
Sample
area |
mg/mL
added |
mg/mL
found |
% Recovery |
% Recovery |
Average |
| 50%_01 |
674.46 |
1159290 |
0.04996 |
0.05454 |
100.1 |
100.1 |
100.1 |
| 50%_02 |
672.90 |
1155954 |
0.04984 |
0.05438 |
100.1 |
100.0 |
| 50%_03 |
673.11 |
1158198 |
0.04986 |
0.05449 |
100.2 |
100.2 |
| 70%_01 |
1018.65 |
1753515 |
0.07545 |
0.08249 |
100.3 |
100.3 |
100.0 |
| 70%_02 |
1018.42 |
1746671 |
0.07544 |
0.08217 |
99.9 |
99.9 |
| 70%_03 |
1016.46 |
1744562 |
0.07529 |
0.08207 |
100.0 |
100.0 |
| 100%_01 |
1349.09 |
2292178 |
0.09993 |
0.10783 |
98.9 |
99.0 |
98.6 |
| 100%_02 |
1348.20 |
2281190 |
0.09987 |
0.10732 |
98.5 |
98.5 |
| 100%_03 |
1347.63 |
2272375 |
0.09982 |
0.10690 |
98.2 |
98.2 |
| 125%_01 |
1686.17 |
2867979 |
0.1249 |
0.13492 |
99.1 |
99.1 |
98.9 |
| 125%_02 |
1685.31 |
2856118 |
0.12484 |
0.13436 |
98.7 |
98.7 |
| 125%_03 |
1685.91 |
2866778 |
0.12488 |
0.13487 |
99.0 |
99.0 |
| 150%_01 |
2015.68 |
3400552 |
0.14931 |
0.15998 |
98.3 |
98.3 |
98.2 |
| 150%_02 |
2023.69 |
3406155 |
0.1499 |
0.16024 |
98.0 |
98.0 |
| 150%_03 |
2021.14 |
3411601 |
0.14971 |
0.16050 |
98.3 |
98.3 |
| Acceptance criteria:% Average recovery shall be between 98.0% -102.0% |
|
