|
|
HPLC |
|
|
|
Spectro |
|
recovery |
|
|
|
|
|
|
|
|
taken |
|
recovery |
|
taken |
|
D1 |
|
DD1 |
|
|
iso |
|
mix |
SAM : FLU ratio |
SAM |
FLU |
SAM |
FLU |
SAM |
FLU |
SAM |
FLU |
SAM at 334 |
SAM at 337.5 |
FLU at 231.5 |
SAM at 343 |
FLU 237.5 |
1 |
1::1 |
100 |
100 |
101.53 |
100.52 |
12 |
12 |
99.54 |
101.04 |
98.14 |
100.37 |
101.05 |
99.44 |
101.84 |
2 |
1::3 |
100 |
300 |
100.93 |
100.58 |
|
|
|
|
|
|
|
|
|
3 |
1::2 |
100 |
200 |
101.19 |
99.61 |
8 |
16 |
99.54 |
102.48 |
101.98 |
102.07 |
100.85 |
101.18 |
100.20 |
4 |
3::2 |
300 |
200 |
100.79 |
101.58 |
12 |
8 |
102.10 |
101.04 |
98.93 |
99.87 |
100.23 |
101.65 |
99.53 |
5 |
2::3 |
200 |
300 |
101.25 |
99.85 |
8 |
12 |
99.72 |
101.04 |
100.60 |
98.17 |
99.61 |
100.23 |
100.24 |
6 |
2::5 |
|
|
|
|
8 |
20 |
99.72 |
101.04 |
102.33 |
98.70 |
100.26 |
99.52 |
100.66 |
7 |
4::3 |
|
|
|
|
16 |
12 |
101.30 |
101.04 |
98.14 |
100.37 |
101.23 |
100.26 |
100.24 |
8 |
4::5 |
|
|
|
|
8 |
20 |
101.43 |
101.48 |
102.08 |
101.97 |
100.26 |
99.40 |
101.01 |
x- |
|
|
|
100.82 |
100.74 |
|
|
100.48 |
101.31 |
100.31 |
100.22 |
100.49 |
100.24 |
100.53 |
±SD |
|
|
|
0.738 |
0.665 |
|
|
1.089 |
0.542 |
1.889 |
1.481 |
0.568 |
0.889 |
0.735 |
%RSD |
|
|
|
0.732 |
0.660 |
|
|
1.084 |
0.535 |
1.883 |
1.478 |
0.565 |
0.887 |
0.731 |
|