HPLC |
|
|
|
%Recovery |
drug taken
(µg\mL) |
|
standard added(µg\mL) |
%Recovery |
|
drug taken
(µg\mL) |
standard added
(µg\mL) |
D1 |
|
DD1 |
|
|
|
ISO |
|
SAM |
FLU |
SAM |
FLU |
SAM |
FLU |
SAM |
FLU |
SAM |
FLU |
SAM |
FLU |
SAM at 334 |
SAM at 337.5 |
FLU 225 |
FLU at 231.5 |
SAM at 343 |
FLU at 237.5 |
100 |
100 |
50 |
50 |
99.00 |
101.92 |
10 |
10 |
4 |
4 |
101.25 |
99.25 |
100.25 |
99.75 |
100.50 |
99.75 |
100.50 |
101.75 |
100 |
100 |
100 |
100 |
101.36 |
100.96 |
10 |
10 |
6 |
6 |
98.50 |
98.17 |
102.00 |
100.33 |
101.83 |
101.00 |
99.67 |
101.50 |
100 |
100 |
150 |
150 |
99.53 |
100.66 |
10 |
10 |
8 |
8 |
101.50 |
100.62 |
99.25 |
99.25 |
98.63 |
99.00 |
99.88 |
98.52 |
x- |
|
|
|
99.96 |
101.09 |
|
|
|
|
100.42 |
99.35 |
100.50 |
99.77 |
100.32 |
99.92 |
100.01 |
100.50 |
± SD |
|
|
|
1.238 |
0.719 |
|
|
|
|
1.665 |
1.230 |
1.392 |
0.542 |
1.612 |
1.010 |
0.438 |
1.952 |
%RSD |
|
|
|
1.238 |
0.711 |
|
|
|
|
1.658 |
1.238 |
1.385 |
0.543 |
1.606 |
1.011 |
0.438 |
1.942 |
|