Analyte Assay (spiking method) Assay in serum
Conc. µgmL-1 %RSD % Rec %RSD %Rec
CAP 8 0.01 99.98 0.002 102
10 0.33 100.04 0.02 101
12 0.36 99.97 0.03 101
MET 8 0.01 100 0.002 101
10 0 100.02 0.002 101.3
12 0.3 99.98 0.02 100.3
PGL 8 0.22 99.3 0.03 100.2
10 0.4 99.98 0.036 100.6
12 99.73 79.79 0.3 101.3
GLB 8 0.01 99.73 0.06 101.3
10 0.3 100.24 0.05 101.6
12 0.5 100.06 0.06 102.0
Table 3: Accuracy of captopril and antidiabetic drugs.