| Condition |
LQC (40.00 ng/mL) |
MQC (600.00 ng/mL) |
HQC (1000.00 ng/mL) |
| Mobile phase: acetonitrile: 5 mM ammonium acetate buffer |
| Negative level (90.1:9.9, v/v) |
39.90 ± 1.39 (3.48%) |
595.43 ± 10.26 (1.72%) |
988.54 ± 14.64 (1.49%) |
| Zero level (90:10, v/v) |
39.93 ± 1.29 (3.23%) |
597.25 ± 14.82 (2.48%) |
996.82 ± 17.35 (1.74%) |
| Positive level (89:10.1, v/v) |
39.91 ± 1.08 (2.71%) |
593.65 ± 12.41 (2.09%) |
995.94 ± 14.76 (1.48%) |
| Flow rate |
| Negative level (0.99 mL/min) |
39.88 ± 1.09 (2.73%) |
596.67 ± 12.57 (2.10%) |
985.87 ± 12.34 (1.57%) |
| Zero level (1.0 mL/min) |
39.92 ± 1.24 (3.10%) |
597.76 ± 13.89 (2.32%) |
994.26 ± 10.46 (1.31%) |
| Positive level (1.01 mL/min) |
39.89 ± 1.15 (2.88%) |
592.39 ± 15.98 (2.69%) |
998.71 ± 15.21 (1.90%) |
|