| Components |
Sample contents
(μg) |
Add quantity
(μg) |
Measured contents
(μg, mean±SD) |
Recovery
() |
RSD
() |
| gamabufotalin |
409.69 |
328 |
743.23±1.00 |
101.69 |
0.13 |
| 410 |
818.71±5.72 |
99.76 |
0.70 |
| 492 |
892.90±8.53 |
98.21 |
0.96 |
| arenobufagin |
144.21 |
116 |
258.94±1.53 |
98.91 |
0.59 |
| 145 |
289.14±3.00 |
99.95 |
1.04 |
| 174 |
317.44±0.94 |
99.56 |
0.30 |
| telocinobufagin |
69.22 |
56 |
125.43±0.44 |
100.38 |
0.35 |
| 70 |
140.00±0.91 |
101.12 |
0.65 |
| 84 |
152.85±1.04 |
99.56 |
0.68 |
| desacetylcinobufotalin |
410.23 |
328 |
737.35±5.53 |
99.73 |
0.75 |
| 410 |
813.20±3.22 |
98.29 |
0.40 |
| 492 |
901.90±6.34 |
99.93 |
0.70 |
| bufotalin |
550.17 |
440 |
987.98±5.28 |
99.5 |
0.53 |
| 550 |
1100.71±9.70 |
100.1 |
0.88 |
| 660 |
1213.61±4.45 |
100.52 |
0.37 |
| cinobufotalin |
128.42 |
102 |
229.02±0.85 |
98.24 |
0.37 |
| 128 |
257.68±0.81 |
100.99 |
0.31 |
| 154 |
279.62±1.82 |
98.44 |
0.65 |
| bufalin |
1619.28 |
1296 |
2912.44±11.29 |
99.78 |
0.39 |
| 1620 |
3213.43±10.98 |
98.4 |
0.34 |
| 1944 |
3552.52±4.07 |
99.45 |
0.11 |
| cinobufagin |
710.31 |
568 |
1274.41±15.65 |
99.31 |
1.23 |
| 710 |
1414.55±3.78 |
99.19 |
0.27 |
| 852 |
1557.59±18.10 |
99.45 |
1.16 |
| resibufogenin |
2332.81 |
1864 |
4184.88±11.26 |
99.36 |
0.27 |
| 2330 |
4659.78±51.33 |
99.87 |
1.10 |
| 2796 |
5115.34±1.45 |
99.52 |
0.03 |
|
