| Parameters |
Alterations |
%RSD for Retention time (n=6) |
|
%RSD for Area (n=6) |
|
%RSD for Assay (n=6) |
|
| |
|
SS |
BH |
ET |
SS |
BH |
ET |
SS |
BH |
ET |
|
Mobile phase |
-2% |
0.2143 |
0.2812 |
0.2018 |
0.2942 |
0.3782 |
0.4871 |
0.2431 |
0.3872 |
0.4321 |
| Normal |
0.2452 |
0.1466 |
0.2167 |
0.2180 |
0.3764 |
0.4813 |
0.2761 |
0.4286 |
0.4982 |
| +2% |
0.1462 |
0.1676 |
0.1972 |
0.2943 |
0.3842 |
0.4319 |
0.3108 |
0.4202 |
0.4874 |
|
Flow rate |
-10% |
0.3113 |
0.4961 |
0.4563 |
0.1278 |
0.4411 |
0.3042 |
0.4532 |
0.4022 |
0.5487 |
| Normal |
0.3871 |
0.5786 |
0.6431 |
0.1132 |
0.5039 |
0.1892 |
0.5431 |
0.4135 |
0.5982 |
| +10% |
0.3217 |
0.6071 |
0.4532 |
0.1484 |
0.4988 |
0.2791 |
0.4596 |
0.5014 |
0.4983 |
|
pH |
-0.2unit |
0.3924 |
0.4254 |
0.5432 |
0.2097 |
0.4373 |
0.3921 |
0.3216 |
0.6165 |
0.6732 |
| Normal |
0.3854 |
0.4711 |
0.5761 |
0.2243 |
0.4828 |
0.4506 |
0.2988 |
0.6746 |
0.6178 |
| +0.2unit |
0.4116 |
0.4582 |
0.5629 |
0.2198 |
0.5498 |
0.5106 |
0.3116 |
0.5153 |
0.6988 |
|
Detection wavelength |
-0.2unit |
0.3132 |
0.6464 |
0.2678 |
0.4173 |
0.5876 |
0.2984 |
0.5473 |
0.3628 |
0.2756 |
| Normal |
0.3201 |
0.6919 |
0.2891 |
0.4442 |
0.5342 |
0.2135 |
0.6759 |
0.3684 |
0.2431 |
| +0.2unit |
0.3091 |
0.5867 |
0.2289 |
0.4892 |
0.5982 |
0.2007 |
0.5192 |
0.3651 |
0.2998 |
|