| Parameters |
Valuesa, SD b, % RSDc |
| System Suitability |
- |
| RT |
4.82 ± 0.02, 0.48 |
| No. of Theoretical Plates |
55316 ± 842.61, 1.52 |
| Tailing Factor |
0.444 ± 0.01, 1.48 |
| Peak purity |
1.00 ± 0.00, 0.00 |
| Capacity factor |
22.44 ± 0.30, 1.32 |
| Linearity |
5-25 µgmL-1 |
| Regression equation |
Y = 20313x + 1687 |
| Correlation coefficient |
0.999 |
| Accuracy |
99.88% ± 0.63, 0.63 |
| Precision |
- |
| Repeatability |
100.04% ± 0.10, 0.10 |
| Intermediate precision |
|
| Day-to-Day |
99.99% ± 0.14, 0.14 |
| Analyst-to-analyst |
99.93% ± 0.10, 0.10 |
| Response ratio |
20523.83 ± 322.68, 1.57 |
| LOQ |
0.206 μg mL-1 ± 0.00, 0.22 |
| LOD |
0.062 μg mx ± 0.00, 0.22 |
| Robustness |
- |
| Formic acid (0.1%) in aqueous content of mobile phase |
99.89% ± 0.21, 0.21 |
| Temperature (± 5%) |
99.97% ± 0.11, 0.11 |
| Specificity |
Ascertained by analyzing standard drug and forced degraded samples |
|
