Parameters Cyp-apo Cyp-CsA
Data collection statistics    
Space group I222 P4212
Unit cell parameters (Å) a,b, c 37.85, 98.20, 111.68 103.97, 103.97, 61.28
Resolution range (Å) 49.08-1.85 (-1.95-1.85) 34.65-1.47 (1.55-1.47)
Measured reflections 75797 (10687) 381226 (50155)
Unique reflections 18133 (2582) 57546 (8279)
Completeness (%) 99.5 (99.5) 99.9 (99.9)
Redundancy 4.2 (4.1) 6.6 (6.1)
Average I/s(I) 9.7 (2.2) 14.2 (2.3)
Rmeas (%) 16.6 (64.9) 9.0 (72.3)
Rsym (%) 14.5 (56.8) 8.3 (66.0)
Refinement statistics    
Reflection in working set 17087 54396
Reflections in test set 868 2759
Rwork/Rfree (%) 17.44/20.50 17.44/20.78
R.m.s.d. bonds (Å) 0.006 0.008
R.m.s.d. angles (º) 1.005 1.857
Ramachandran plot (%)    
Favored 96.30 96.01
Allowed 3.70 3.38
Disallowed 0 0.61
The values in parentheses refer to statistics in the highest bin.
Table 1: Data collection and refinement statistics.