Samples |
Quantities of samples |
HNO3
(mL) |
H2O2
(mL) |
Digestion program |
|
Steps |
Time
(min) |
Power
(W) |
Temperature
(ºC) |
References |
Coffee powder |
300 (mg) |
7 |
1 |
1 |
5 |
750 |
120 |
45 |
(n=4) |
|
|
2 |
3 |
750 |
120 |
|
|
|
3 |
10 |
750 |
210 |
|
|
|
4 |
15 |
750 |
210 |
Coffee infusion* |
2 (mL) |
5 |
1 |
1 |
5 |
400 |
80 |
46 |
(n=4) |
|
|
2 |
5 |
400 |
120 |
|
|
|
3 |
5 |
400 |
210 |
Rat livers
and diets |
300 (mg) |
6 |
2 |
1 |
3 |
250 |
130 |
46 |
(n=4) |
|
|
2 |
5 |
630 |
130 |
|
|
|
3 |
22 |
500 |
130 |
|
|
|
4 |
15 |
0 |
130 |
|
*All infusion volumes were reduced to 1/4 of the initial volume. |
Table 1: Conditions of digestion program used in coffee samples, rat livers and diets. |