| No |
δH (J in Hz) |
δC |
δH (J in Hz) |
δC |
δH (J in Hz) |
δC |
| 1α |
1.22,m |
38.05 |
0.99,m |
39.56 |
4.22, dd, 11.1, 5.0 |
69.87 |
| 1β |
1.88,m |
- |
1.82,m |
- |
- |
- |
| 2α |
1.96,m |
35.67 |
1.62,m |
20.12 |
1.99,m |
21.62 |
| 2β |
2.04,m |
- |
1.75,m |
- |
1.68,m |
- |
| 3α |
4.68, dd, 11.5, 5.0 |
76.32 |
1.45,m |
32.67 |
1.36,m |
39.51 |
| 3β |
- |
- |
1.88,m |
- |
1.27,m |
- |
| 4 |
- |
53.1 |
- |
42.18 |
- |
- |
| 5 |
2.21, brd, 12.3 |
53.76 |
1.50, d, 11.5 |
60.01 |
1.60,m |
60.31 |
| 6α |
1.60,m |
20.31 |
4.21, t, 11.5 |
76.11 |
4.22, t, 11.5 |
76.18 |
| 6β |
1.87,m |
- |
- |
- |
- |
- |
| 7α |
2.92,m |
30.42 |
- |
69.98 |
2.06.m |
34.56 |
| 7β |
2.80,m |
- |
4.15, t, 3.0 |
- |
2.67,m |
- |
| 8 |
- |
131.56 |
2.56,m |
38.17 |
1.58,m |
38.32 |
| 9 |
- |
142.73 |
1.22,m |
37.19 |
1.26,m |
36.93 |
| 10 |
- |
38.67 |
- |
35.98 |
- |
36.1 |
| 11α |
7.29, d, 8.5 |
127.92 |
1.90,m |
20.32 |
1.94,m |
19.03 |
| 11β |
- |
- |
1.70,m |
- |
1.68,m |
- |
| 12α |
7.17, d, 8.5 |
126.12 |
1.78,m |
36.71 |
1.74,m |
35.78 |
| 12β |
- |
- |
1.50,m |
- |
1.59,m |
- |
| 13 |
- |
144.21 |
- |
36.23 |
- |
35.63 |
| 14α |
6.85,s |
129.48 |
1.68, bd, 13.5 |
39.19 |
1.70, bd, 13.5 |
40.11 |
| 14β |
- |
- |
1.59, d, 13.5 |
- |
1.60, d, 13.5 |
- |
| 15 |
3.05, sept, 7.0 |
34.52 |
5.90, dd, 10.6, 17.8 |
146.12 |
5.91, dd, 10.6, 17.8 |
146.24 |
| 16 |
0.87, d, 7.0 |
28.03 |
4.78, cis: dd, 5.11, d, 10.6 4.92, trans: 5.15, d, 17.8 |
112.43 |
4.77, cis: dd, 5.11, d, 10.6 4.92, trans: 5.15, d, 17.8 |
111.56 |
| 17 |
0.87, d, 7.0 |
28.03 |
0.83,s |
24.12 |
0.88,s |
26.43 |
| 18 |
1.29,s |
23.59 |
- |
179.74 |
- |
177.9 |
| 19 |
4.07, d,11.6 3.56, d, 11.5 |
68.32 |
1.21,s |
16.73 |
0.93,s |
17.32 |
| 20 |
1.25,s |
25.48 |
0.86,s |
18.76 |
0.90,s |
18.75 |
| CH3CO |
2.12,s |
21.32 |
2.16,s |
22.01 |
2.09,s |
21.98 |
| CH3CO |
- |
167.45 |
- |
170.33 |
- |
172.43 |
|