| Column |
ZB-5MS, 30 m × 0.25 mm × 0.25 µm |
| Injector temperature |
150°C |
| Carrier gas |
Helium |
| Carrier gas flow |
1.0 mL/min |
| Split ratio |
5:00 |
| Oven Programme |
40°C, 4.0 min |
| |
20.0°C/min 200°C 13.00 min |
| |
Total run time: 25.0 min |
| Injection Volume |
1.0 µL |
| Diluent |
Dichloro Methane |
| MS Parameters: |
| Ionisation source |
EI |
| Electron energy |
70 Ev |
| Source temperature |
280°C |
| Interface Temperature |
260°C |
| SIM or SIR (Selective Ion Monitoring) Parameters: |
| m/z fragment |
79 |
| Solvent Cut time |
3.0 min |
| Detector Voltage |
0.92 KV |
| Start Time |
3.01 min |
| End time |
8.0 min |
|
