Mycotoxins Conc. Range (µg Kg−1) Repeatabilitya
R ± RSDr (%)
Reproducibilitya
R ± RSDR (%)
LOD (µg Kg−1) LOQ (µg Kg−1)
Aflatoxin B1 0.25 – 16.0            103.7 ± 5.1 (0.5), 103.6 ± 8.1 (1.0)    101.0 ± 8.1 (2.0) 0.16 0.52
Aflatoxin B2 0.25 – 16.0 100.0 ± 6.7 (0.5), 101.5 ± 6.1 (1.0)    99.8 ± 3.8 (2.0) 0.15 0.5
Aflatoxin G1 0.25 – 16.0   112.3 ± 8.1 (0.5), 105.5 ± 7.5 (1.0)    104.6 ± 3.7 (2.0) 0.17 0.56
Aflatoxin G2 0.25 – 16.0 91.3 ± 7.3 (0.5)  102.7 ± 7.0 (2.0) 0.14 0.46
Ochratoxin A 0.4 – 32.0 113.0 ± 4.7 (0.5), 96.4 ± 4.4 (1.5)    103.8 ± 4.1 (3.0) 0.17 0.56
Fumonisin B1 5.0 – 640 52.8 ± 3.3 (10.0), 88.9 ± 6.0 (1000)    82.2 ± 7.3 (500) 1.6 5.3
Fumonisin B2 5.0 – 640 66.2 ± 1.5 (10.0), 120.4 ± 3.2 (200)    98.1 ± 4.7 (500) 2 6.6
Zearalenone 5.0 – 640 110.5 ± 2.7 (10.0), 112.7 ± 6.9 (35.0)    101.9 ± 4.4 (75.0) 3.4 11.1
Deoxynivaleno1     5.0 – 800 104.6 ± 2.3 (25.0), 102.6 ± 2.4 (450)    99.7 ± 2.1 (760) 7.9 26.2
T-2 toxin 5.0 – 800 107.7 ± 9.6 (25.0), 96.6 ± 12.6 (40.0)    112.0 ± 11.1 (50.0) 8.2 26.9
aSpiking levels (µg Kg−1) are given in the brackets
Table 3: Average recovery values (R), relative standard deviation (RSD), LODs and LOQs (µg Kg−1) obtained for the eleven mycotoxins in wheat.