| |
Temp(°C) |
RampTime(s) |
HoldTime(s) |
Internal Flow(mL/min) |
| Mg2+ 5 µL injection volume |
| drying |
80 |
1 |
30 |
250 |
| drying |
120 |
15 |
60 |
250 |
| drying |
500 |
40 |
30 |
250 |
| pyrolysis |
900 |
10 |
20 |
250 |
| atomization |
1900 |
0 |
5 |
0 |
| clean |
2450 |
1 |
3 |
250 |
| K+ 5 µL injection volume |
| drying |
110 |
1 |
30 |
250 |
| drying |
130 |
15 |
30 |
250 |
| pyrolysis |
900 |
10 |
20 |
250 |
| atomization |
1500 |
0 |
5 |
0 |
| clean |
2450 |
1 |
3 |
250 |
|
