| Position |
1
δH (mult, J/Hz) δC |
2
δH (mult, J/Hz) δC |
| 1 |
0.86 m, 1.87 m |
41.2 |
0.85 m, 1.87 m |
41.3 |
| 2 |
1.40 m, 1.90 m |
20.3 |
1.42 m, 1.95 m |
20.3 |
| 3 |
1.06 m, 2.25 m |
38.3 |
1.06 m, 2.23 m |
38.5 |
| 4 |
|
43.7 |
|
44.7 |
| 5 |
1.08 m |
58.2 |
1.09 m |
58.3 |
| 6 |
1.88 m, 1.94 m |
22.6 |
1.86 m, 1.98 m |
22.6 |
| 7 |
1.43 m, 1.55 m |
42.5 |
1.42 m, 1.58 m |
42.5 |
| 8 |
|
43.1 |
|
43.3 |
| 9 |
0.98 m |
54.9 |
0.99 m |
54.7 |
| 10 |
|
39.5 |
|
39.9 |
| 11 |
1.62 m, 1.78 m |
21.1 |
1.64 m, 1.82 m |
21.1 |
| 12 |
1.52 m, 1.96 m |
38.0 |
1.48 m, 2.01 m |
38.0 |
| 13 |
|
87.8 |
|
87.8 |
| 14 |
1.54 m, 2.24 m |
44.6 |
1.61 m, 2.26 m |
45.2 |
| 15 |
1.94 m, 2.10 m |
47.8 |
2.01 m, 2.19 m |
48.5 |
| 16 |
|
154.4 |
|
154.4 |
| 17 |
4.84 s, 5.25 s |
105.3 |
4.84 m, 5.14 m |
105.3 |
| 18 |
1.22 s |
28.8 |
1.24 s |
29.0 |
| 19 |
|
178.5 |
|
178.5 |
| 20 |
0.95 s |
17.1 |
0.93 s |
16.6 |
| 1′ |
5.50 d (8.5) |
94.2 |
5.55 d (7.8) |
93.8 |
| 2′ |
3.62 m |
80.0 |
3.79 m |
79.8 |
| 3′ |
3.46 m |
78.1 |
3.58 m |
77.9 |
| 4′ |
3.32 m |
71.2 |
3.32 m |
71.4 |
| 5′ |
3.35 m |
78.0 |
3.35 m |
78.2 |
| 6′ |
3.60 m, 3.82 m |
62.1 |
3.56 m, 3.79 m |
62.3 |
| 1′′ |
4.70 d (8.2) |
96.6 |
4.65 d (8.2) |
98.0 |
| 2′′ |
3.57 m |
80.4 |
3.57 m |
79.3 |
| 3′′ |
3.93 m |
87.4 |
3.76 m |
88.8 |
| 4′′ |
3.36 m |
70.2 |
3.45 m |
71.2 |
| 5′′ |
3.28 m |
77.3 |
3.28 m |
77.6 |
| 6′′ |
3.64 m, 3.80 m |
62.5 |
3.56 m, 3.78 m |
62.8 |
| |
|
|
|
|
| 1′′′ |
4.86 d (7.8) |
103.7 |
5.42 d (1.2) |
101.8 |
| 2′′′ |
3.24 m |
75.6 |
3.84 m |
71.8 |
| 3′′′ |
3.32 m |
78.1 |
3.62 m |
72.0 |
| 4′′′ |
3.13 m |
71.6 |
3.49 m |
73.6 |
| 5′′′ |
3.44 m |
77.9 |
3.82 m |
70.0 |
| 6′′′ |
3.56 m, 3.80 m |
63.1 |
1.24 d (6.3) |
18.1 |
| 1′′′′ |
4.74 d (7.8) |
103.8 |
4.50 d (7.4) |
104.1 |
| 2′′′′ |
3.27 m |
75.3 |
3.25 m |
75.1 |
| 3′′′′ |
3.42 m |
78.5 |
3.42 m |
78.6 |
| 4′′′′ |
3.32 m |
71.3 |
3.32 m |
71.1 |
| 5′′′′ |
3.36 m |
78.1 |
3.36 m |
77.8 |
| 6′′′′′ |
3.62 m, 3.84 m |
62.3 |
3.60 m, 3.80 m |
62.4 |
| 1′′′′′ |
4.72 d (7.4) |
104.6 |
4.71 d (8.2) |
104.3 |
| 2′′′′′ |
3.29 m |
71.6 |
3.19 m |
74.9 |
| 3′′′′′ |
3.28 m |
72.2 |
3.36 m |
75.4 |
| 4′′′′′ |
3.02 t (8.9) |
77.0 |
3.34 m |
71.6 |
| 5′′′′′ |
3.27 m |
70.4 |
3.42 m |
74.6 |
| 6′′′′′ |
1.28 d (6.3) |
17.9 |
3.48 m, 3.76 m |
62.2 |
aassignments made on the basis of COSY, 1D TOCSY, HSQC and HMBC
correlations |
