Conc.
μg mL-1 |
Day 1 (% Recovery) |
Day 2 (% Recovery) |
Day 3 (% Recovery) |
| |
PRZ |
AML |
DIL |
VER |
PRZ |
AML |
DIL |
VER |
PRZ |
AML |
DIL |
VER |
| API |
|
|
|
|
|
|
|
|
|
|
|
|
| 5 |
99.28 |
99.79 |
100.2 |
100.0 |
99.98 |
99.25 |
101.2 |
100.5 |
99.52 |
99.82 |
100.5 |
100.3 |
| 10 |
99.93 |
100.1 |
100.1 |
99.94 |
99.85 |
98.99 |
100.2 |
99.24 |
99.74 |
99.51 |
99.58 |
98.83 |
| 15 |
98.95 |
100.0 |
99.81 |
99.58 |
100.2 |
98.74 |
100.5 |
100.7 |
99.94 |
99.29 |
100.1 |
100.2 |
| 20 |
99.71 |
99.60 |
98.59 |
99.90 |
99.65 |
99.68 |
99.87 |
99.83 |
99.28 |
100.7 |
99.58 |
99.57 |
| 25 |
100.2 |
100.5 |
99.96 |
100.3 |
98.59 |
99.89 |
100.7 |
99.17 |
99.51 |
99.59 |
101.2 |
98.46 |
| 50 |
100.7 |
99.28 |
100.2 |
100.6 |
100.2 |
100.1 |
100.0 |
100.5 |
100.0 |
99.87 |
99.51 |
100.1 |
| 100 |
99.97 |
98.89 |
100.1 |
99.08 |
99.87 |
99.05 |
99.96 |
100.9 |
99.57 |
99.26 |
99.27 |
99.87 |
| Serum |
| 5 |
100.0 |
99.28 |
99.86 |
99.95 |
100.2 |
99.16 |
100.8 |
100.2 |
99.01 |
99.51 |
100.2 |
100.1 |
| 10 |
99.65 |
99.58 |
100.0 |
100.1 |
100.5 |
98.58 |
100.4 |
9.65 |
99.97 |
99.01 |
100.7 |
99.28 |
| 15 |
99.18 |
99.71 |
99.67 |
100.8 |
100.8 |
98.11 |
100.2 |
100.4 |
98.28 |
99.64 |
99.96 |
99.17 |
| 20 |
99.50 |
99.83 |
99.58 |
99.92 |
99.85 |
99.19 |
100.1 |
99.92 |
99.87 |
98.17 |
99.57 |
99.51 |
| 25 |
99.68 |
100.1 |
100.0 |
100.2 |
99.69 |
99.38 |
100.9 |
99.75 |
100.2 |
99.84 |
101.0 |
100.1 |
| 50 |
99.98 |
99.05 |
99.68 |
100.6 |
99.53 |
99.82 |
99.58 |
100.1 |
99.17 |
99.63 |
99.15 |
99.47 |
| 100 |
99.37 |
99.18 |
101.0 |
99.87 |
99.08 |
98.95 |
100.2 |
100.4 |
98.96 |
99.50 |
100.0 |
99.96 |
|