Potentiometric Titration of Paracetamol in glacial acetic acid with 0.1 N HCIO4 in glacial acetic acid, using platinum - calomel electrodes |
Volume of 0.1 N HCIO4, ml |
Potential,Volts |
Volume of 0.1 N HCIO4, ml |
Potential,Volts |
5 |
0.49 |
15 |
0.525 |
5.5 |
0.49 |
16 |
0.525 |
6 |
0.49 |
17 |
0.53 |
7 |
0.49 |
18 |
0.53 |
8 |
0.495 |
19 |
0.53 |
9 |
0.5 |
20 |
0.535 |
10 |
0.5 |
21 |
0.535 |
11 |
0.504 |
22 |
0.535 |
12 |
0.514 |
23 |
0.535 |
13 |
0.514 |
24 |
0.535 |
14 |
0.525 |
25 |
0.535 |
Potentiometric Titration of Paracetamol in pyridine with 0.075 N soldiumethoxide in ethyl alcohol, using platinum – calomel electrodes |
Volume of 0.075 N C2H5ONa, ml |
Potential, Volts |
Volume of 0.075 N C2H5ONa, ml |
Potential, Volts |
4 |
0.22 |
15 |
0.279 |
5 |
0.22 |
16 |
0.293 |
6 |
0.225 |
17 |
0.305 |
7 |
0.225 |
18 |
0.314 |
8 |
0.232 |
19 |
0.317 |
9 |
0.232 |
20 |
0.317 |
10 |
0.232 |
21 |
0.326 |
11 |
0.239 |
22 |
0.326 |
12 |
0.243 |
23 |
0.326 |
13 |
0.249 |
24 |
0.326 |
14 |
0.26 |
25 |
0.326 |
Potentiometric Titration of Paracetamol in dimethylformamide with 0.075 N sodium ethoxide in ethyl alcohol, using platinum-calomel electrodes. |
Volume of 0.075 N C2H5ONa, ml |
Potential, Volts |
Volume of 0.075 N C2H5ONa, ml |
Potential, Volts |
2 |
0.22 |
17 |
0.262 |
3 |
0.224 |
18 |
0.273 |
4 |
0.227 |
19 |
0.28 |
5 |
0.227 |
20 |
0.282 |
6 |
0.227 |
21 |
0.285 |
7 |
0.227 |
22 |
0.288 |
8 |
0.227 |
23 |
0.291 |
9 |
0.227 |
24 |
0.291 |
10 |
0.223 |
25 |
0.291 |
11 |
0.223 |
26 |
0.291 |
12 |
0.223 |
27 |
0.291 |
13 |
0.226 |
28 |
0.291 |
14 |
0.231 |
29 |
0.291 |
15 |
0.235 |
30 |
0.291 |
16 |
0.247 |
|
|
Potentiometric Titration of Paracetamol in Pyridine with 0.09 N sodium ethoxide in ethyl alcohol. |
Volume of 0.09 N C2H5ONa, ml |
Potential, Volts |
Volume of 0.09 N C2H5ONa, ml |
Potential, Volts |
3 |
0.385 |
15 |
0.415 |
4 |
0.385 |
16 |
0.415 |
5 |
0.385 |
17 |
0.42 |
6 |
0.385 |
18 |
0.42 |
7 |
0.385 |
19 |
0.42 |
8 |
0.395 |
20 |
0.42 |
9 |
0.395 |
21 |
0.42 |
10 |
0.395 |
22 |
0.42 |
11 |
0.4 |
23 |
0.42 |
12.1 |
0.405 |
24 |
0.42 |
13 |
0.415 |
25 |
0.42 |
14 |
0.415 |
|
|
Potentiometric Titration of Paracetamol in dimethyl formamide with 0.09 N sodium ethoxide in ethylalcohol. |
Volume of 0.09 N C2H5ONa, ml |
Potential, Volts |
Volume of 0.09 N C2H5ONa, ml |
Potential, Volts |
0.5 |
0.395 |
13 |
0.415 |
1 |
0.395 |
14 |
0.42 |
2 |
0.395 |
15 |
0.42 |
3 |
0.395 |
16 |
0.42 |
4 |
0.395 |
17 |
0.42 |
5 |
0.395 |
18 |
0.42 |
6 |
0.395 |
19 |
0.42 |
7 |
0.395 |
20 |
0.42 |
8 |
0.4 |
21 |
0.42 |
9 |
0.4 |
22 |
0.42 |
10 |
0.4 |
23 |
0.42 |
11 |
0.405 |
24 |
0.42 |
12 |
0.405 |
25 |
0.42 |
pH-metric Titration of Paracetamol in ethyl alcohol with 0.083 N sodium ethoxide in ethylalcohol. |
Volume of 0.083 N C2H5ONa, ml |
pH |
Volume of 0.083 N C2H5ONa, ml |
Potential, Volts |
4 |
12 |
14.5 |
13.3 |
5 |
12.1 |
15 |
13.4 |
6 |
12.15 |
16 |
13.5 |
7 |
12.25 |
17 |
13.6 |
7.5 |
12.3 |
18 |
13.65 |
8 |
12.4 |
19 |
13.7 |
9 |
12.5 |
20 |
13.75 |
10 |
12.6 |
21 |
13.75 |
11 |
12.7 |
22 |
13.8 |
12 |
12.8 |
23 |
13.8 |
13 |
12.9 |
24 |
13.8 |
14 |
13.2 |
25 |
13.85 |
|