| Research Article |
Open Access |
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| Synthesis of Polyfunctional Organic Systems Containing
1- Acyl / Aroyl - anilido-butadienes and their uses as
Photochemical Probes and Chelating Agents for Removal of
Bismuth (III) from Industrial Wastewater |
| M. S. T. Makki1*, R. M. Abdel-Rahman and M. S. El-Shahawi2 |
1Department of Chemistry, Faculty of Science, King Abdulaziz University, P. O. Box 80203 Jeddah 21589, Kingdom of Saudi Arabia
2Department of Chemistry, Faculty of Science at Damiatta, Mansoura University, Mansoura, Egypt |
| *Corresponding author: |
Dr. M. S. T. Makki
Department of Chemistry
Faculty of
Science
King Abdulaziz University
P. O. Box 80203
Jeddah 21589, Kingdom of
Saudi Arabia
Tel: 00-9662-6952000
Fax: 00-9662-6952292
E-mail: mmakki @
kau.edu.sa |
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| Received July 06, 2010; Accepted August 21, 2010; Published August 21, 2010 |
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| Citation: Makki MST, Abdel-Rahman RM, El-Shahawi MS (2010) Synthesis of
Polyfunctional Organic Systems Containing 1- Acyl / Aroyl - anilido-butadienes and
their uses as Photochemical Probes and Chelating Agents for Removal of Bismuth
(III) from Industrial Wastewater. J Bioanal Biomed 2: 085-090. doi:10.4172/1948-
593X.1000028 |
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| Copyright: © 2010 Makki MST, et al. This is an open-access article distributed
under the terms of the Creative Commons Attribution License, which permits
unrestricted use, distribution, and reproduction in any medium, provided the
original author and source are credited.
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| Abstract |
The present article reports the synthesis of a series of some new 1-acyl/ benzoyl -1-anilido-4-methyl /aryl-1,
3-butadiene derivatives (II - IV) by warming primary heteroamines and/ or sulfa drugs with pre heated ethyl acetoacetate
and / or ethyl benzoylacetate in dry conditions followed by condensation with unsaturated aromatic aldehydes in
boiling ethanol-piperidine. The chemical structures of the compounds were characterized via their elemental analysis
and spectroscopic measurements (UV Vis., IR, 1HNMR). Some of the compounds (IIId, e, f, IV d, e,f) were tested as
antimicrobial and photochemical probe agents. Compound IVa was physically loaded onto polyurethane solid sorbent
and successfully used for the removal and / or pre concentration of bismuth (III) from industrial wastewater. The
voltammetric behavior of the two compounds IIa and IVa in N, N-dimethylformamide was investigated.
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