| C. No |
δC |
δH/ppm (multi, integral, J/Hz) |
HMBC |
| 1 |
33.8 |
2.23 (1H, s) |
C3,C5 |
| |
|
1.82 (1H, m) |
C4, C10 |
| 2 |
25.6 |
2.01 (1H, m) |
|
| |
|
1.18 (1H, m) |
|
| 3 |
77.9 |
3.43 (IH, dd, 10.5 and 4.0) |
|
| 4 |
37.3 |
|
|
| 5 |
55.7 |
2.03(1H, m) |
C8, C10 |
| 6 |
18.7 |
1.65(1H, d, 3.6) |
|
| |
|
1.45 (1H, d, 3.0) |
C5, C9, C14 |
| 7 |
33.4 |
1.46 (1H, m) |
|
| |
|
1.34 (1H, m) |
|
| 8 |
39.6 |
|
|
| 9 |
47.8 |
1.57 (1H, m) |
|
| 10 |
35.4 |
|
|
| 11 |
23.7 |
1.84 (1H, m) |
C8, C13 |
| |
|
1.20 (1H, m) |
|
| 12 |
124.9 |
|
|
| 13 |
140.5 |
|
|
| 14 |
39.5 |
|
|
| 15 |
28.1 |
1.80 (1H, m) |
|
| 16 |
24.6 |
0.99 (1H, m) |
C14, C18 |
| |
|
1.57 (1H, m) |
|
| 17 |
42.6 |
|
|
| 18 |
43.3 |
0.85 (1H, s) |
C14, C16 |
| 19 |
83.1 |
4.13 (1H, d, 5.4) |
|
| 20 |
39.3 |
|
|
| 21 |
40.3 |
1.95 (1H, m) |
|
| |
|
1.47 (1H, m) |
|
| 22 |
39.1 |
1.63 (1H, m) |
|
| |
|
1.52 (1H, m) |
|
| 23 |
16.6 |
1.04 (3H, s) |
C3, C5 |
| 24 |
28.7 |
1.22 (3H, s) |
C3, C5 |
| 25 |
15.8 |
0.94 (3H, s) |
C1,C 9 |
| 26 |
21.2 |
1.21 (3H, s) |
C9, C14 |
| 27 |
24.0 |
1.07 (3H, s) |
C7, C15 |
| 28 |
24.8 |
0.80 (3H, s) |
C16, C22 |
| 29 |
182.3 |
|
|
| 30 |
17.1 |
0.90 (3H, s) |
C19, C21, C29 |
|
