alexa Synthesis of Pyramid-Shaped NiO Nanostructures using Low-Temperature Composite- Hydroxide- Mediated Approach

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Synthesis of Pyramid-Shaped NiO Nanostructures using Low-Temperature Composite- Hydroxide- Mediated Approach

Composite-hydroxide-mediated (CHM) approach was used to synthesize NiO nanocrystals. The proposed method makes use of molten composite hydroxides; providing reaction media and lower the process temperature. Processing temperature and reaction time are the two potential parameters to control the growth of a nanomaterial. The method was used at temperatures in the range of 180-250°C and formation of the nanomaterial was monitored using XRD, SEM, EDX, FTIR, and UV-visible spectroscopy. The produced nanomaterial was purely polycrystalline with an average crystallite size in the range of 23.71-36.92 nm. Method suggested formation of pyramid shaped NiO nanocrystals in the temperature range 220-250°C. To know more

 
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