alexa Binary Titanium (IV) Metal-organic Frameworks with Multidentate Ligands | OMICS International
ISSN: 2161-0401

Organic Chemistry: Current Research
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Research Article

Binary Titanium (IV) Metal-organic Frameworks with Multidentate Ligands

Balram Prasad Baranwal*, Abhay Kumar Jain and Alok Kumar Singh
Coordination Chemistry Research Laboratory, Department of Chemistry, D.D.U. Gorakhpur University, Gorakhpur 273 009, India
Corresponding Author : Balram Prasad Baranwal
Coordination Chemistry Research Laboratory
Department of Chemistry, D.D.U. Gorakhpur University
Gorakhpur 273009, India
Tel: +91 551 2203459
E-mail: [email protected]
Received November 07, 2011; Accepted November 25, 2011; Published November 27, 2011
Citation: Baranwal BP, Jain AK, Singh AK (2011) Binary Titanium (IV) Metalorganic Frameworks with Multidentate Ligands. Organic Chem Current Res S3:001. doi: 10.4172/2161-0401.S3-001
Copyright: © 2011 Baranwal BP, et al. This is an open-access article distributed under the terms of the Creative Commons Attribution License, which permits unrestricted use, distribution, and reproduction in any medium, provided the original author and source are credited.

Abstract

Some volatile binary metal-organic frameworks of titanium (IV), [Ti(OOCR) 4 ] (where R = C 13 H 27, C 15 H 31, C 17 H 35 or C 21 H 43 ) were synthesized by the reaction of titanium tetrachloride and sodium salts of the straight chain fatty acids (prepared in situ) in 1:4 molar ratio. The isolated solid products were showing poor crystallinity and were characterized by their elemental analyses, molecular weight determinations, conductance, spectral (infrared, 1 H NMR, 13 C NMR, FAB mass and powder XRD) and TEM studies. Their monomeric nature was confirmed by molecular weight determinations and FAB mass spectra. Eight coordination number of titanium (IV) have been assigned in the isolated compounds. TEM indicated the particles are spherical in shape having ~200 nm diameter.

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