alexa Mesoporous Zr-MCM-41 and Ti-MCM-41 as Solid Oxidation C
ISSN ONLINE(2319-8753)PRINT(2347-6710)

International Journal of Innovative Research in Science, Engineering and Technology
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Research Article

Mesoporous Zr-MCM-41 and Ti-MCM-41 as Solid Oxidation Catalysts in the synthesis of Epichlorohydrin

Shrinivas Ghodke1, Rajesh Patel1 and Uma Chudasama2*
  1. Research Scholar, Department of Applied Chemistry, Faculty of Technology & Engineering, The M. S. University of Baroda, Vadodara, Gujarat, India.
  2. Professor, Department of Applied Chemistry, Faculty of Technology & Engineering, The M. S. University of Baroda, Vadodara, Gujarat, India.
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Abstract

Mesoporous Zr-MCM-41 and Ti-MCM-41 have been synthesized at room temperature by sol-gel method using templates possessing high surface area, good thermal stability and maximum M4+ incorporation varying SiO2:ZrO2/TiO2 ratios. The salient feature is synthesis of the materials at room temperature. Both the synthesized materials have been characterized for elemental analysis by ICP-AES, XRD, TEM, SEM, EDX, surface area (by BET method), pore volume and pore distribution (BJH method), UV-DRS, FTIR and TGA. Further, the catalytic potential of both the materials have been compared by studying epoxidation as a model reaction using H2O2 as an oxidant in the conversion of allyl chloride to selectively produce epichlorohydrin in a single step at room temperature by varying several parameters such as catalyst amount, reaction time, types of oxidants including catalyst regeneration and reuse.

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