alexa Separation/Analysis of Chrysophanol by Ionic Liquid Loaded β-Cyclodextrin Polymer Coupled with Ultraviolet Spectrophotometry
ISSN: 2161-1009

Biochemistry & Analytical Biochemistry
Open Access

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Research Article

Separation/Analysis of Chrysophanol by Ionic Liquid Loaded β-Cyclodextrin Polymer Coupled with Ultraviolet Spectrophotometry

Wenhui Ping, Hongyan Xu and Xiashi Zhu*

College of Chemistry and Chemical Engineering, Yangzhou University, China

*Corresponding Author:
Xiashi Zhu
College of Chemistry and
Chemical Engineering
Yangzhou University, China
Tel: +86-514-7975244
E-mail: [email protected]

Received Date: August 21, 2013; Accepted Date: September 16, 2013; Published Date: September 19, 2013

Citation: Ping W, Xu H, Zhu X (2013) Separation/Analysis of Chrysophanol by Ionic Liquid Loaded β-Cyclodextrin Polymer Coupled with Ultraviolet Spectrophotometry. Biochem Anal Biochem 2:138. doi: 10.4172/2161-1009.1000138

Copyright: © 2013 Ping W. This is an open-access article distributed under the terms of the Creative Commons Attribution License, which permits unrestricted use, distribution, and reproduction in any medium, provided the original author and source are credited.

Abstract

A novel method for separation/analysis of chrysophanol (Chry) in drugs is described. The work is based on the utilization of ionic liquid ([C4min] PF6) (IL) loaded β-cyclodextrin cross-linked polymer (IL-β-CDCP) for effective adsorption of Chry coupled with ultraviolet spectrophotometry for the analysis of Chry. The inclusion interaction of IL-β-CDCP with Chry is studied by FTIR and 13C-NMR. Under the optimum conditions, linear range, Detection Limit (DL) and the relative standard deviation are 0.10-20.0 μg mL-1, 0.02 μg mL-1, 0.45% (n=3, c=4.0 μg mL-1), respectively. This technique is successfully applied for determination of Chry in drug samples.

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