alexa Conventional and Microwave-hydrothermal Synthesis of TiO2Nanopowders.
Materials Science

Materials Science

Research & Reviews: Journal of Material Sciences

Author(s): Anna Bonamartini Corradi, Federica Bondioli, Bonaventura Focher, Anna Maria Ferrari

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The objective of this study was to compare the conventional and microwave hydrothermal treatment of TiOCl2 solutions. Colloidal titania suspensions were prepared by forced hydrolysis at 195°C for different times ranging from 1 to 32 h for the conventional synthesis and from 5 min to 1 h for the microwave ones. The effect of the microwave technology on both the synthesis conditions and titania nanoparticles properties has been evaluated. Particles morphology and crystallinity were studied by using transmission electron microscopy and X-ray diffraction. The thermal and chemical stability of the obtained powders were determined by TG/DTA analysis.

This article was published in J Am Ceram Soc and referenced in Research & Reviews: Journal of Material Sciences

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