alexa Extraction and Preconcentration of N-Tolyl-Sulfonyl-Phosphoramid- Saeure-Dichlorid as an Anti-Cancer Drug from Plants: A Pharmacognosy Study
Oncology

Oncology

Chemotherapy: Open Access

Author(s): A Heidari

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In the present Editorial, a new and rapid Headspace Solvent Micro Extraction (HSME) method is utilized, for the extraction and preconcentration of the volatile and anti– cancer compounds such as N-Tolyl-Sulfonyl-Phosphoramid-Saeure-Dichlorid from plant samples into a microdrop [1-9]. The extraction occurred by suspending a microdrop of the solvent from the tip of a micro syringe to the headspace of the dried and powdered plants samples in a sealed vial for a preset extraction time [10-15]. Then, the microdrop was retracted back into the micro syringe and injected directly into a Gas Chromatography (GC) injection port (equipped with a Flame Ionization Detector (FID)). The identification of the volatile and anti- cancer compounds extracted by Headspace Solvent Micro Extraction (HSME) was confirmed according to their retention indices and mass spectra (EI, 150 eV) and quantitative analysis was performed by Gas Chromatography–Flame Ionization Detector (GC-FID). Parameters such as the sample temperature, micro syringe needle temperature, sample volume, extraction time and microdrop volume were studied and optimized in ten levels and finally, the method performance was evaluated

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This article was published in A Pharmacognosy Study. J Pharmacogn Nat Prod and referenced in Chemotherapy: Open Access

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