alexa Forced degradation and impurity profiling: recent trends in analytical perspectives.
Chemical Engineering

Chemical Engineering

Journal of Chromatography & Separation Techniques

Author(s): Jain D, Basniwal PK, Jain D, Basniwal PK

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Abstract This review describes an epigrammatic impression of the recent trends in analytical perspectives of degradation and impurities profiling of pharmaceuticals including active pharmaceutical ingredient (API) as well as drug products during 2008-2012. These recent trends in forced degradation and impurity profiling were discussed on the head of year of publication; columns, matrix (API and dosage forms) and type of elution in chromatography (isocratic and gradient); therapeutic categories of the drug which were used for analysis. It focuses distinctly on comprehensive update of various analytical methods including hyphenated techniques for the identification and quantification of thresholds of impurities and degradants in different pharmaceutical matrices. © 2013 Elsevier B.V. All rights reserved. This article was published in J Pharm Biomed Anal and referenced in Journal of Chromatography & Separation Techniques

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