alexa Liquid chromatography mass spectrometry of fatty acids as their anilides.
Toxicology

Toxicology

Journal of Environmental & Analytical Toxicology

Author(s): Kusaka T, Ikeda M, Nakano H, Numajiri Y

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Abstract The mass spectra of a series of saturated (C16:0-C30:0) and unsaturated (C16:1, C18:1, C18:2, C18:3) fatty acids have been recorded as their anilides using liquid chromatography/mass spectrometry with the atmospheric-pressure-ionization interface system. The spectra show an intense peak for (molecule + H)+ ion in each case. The liquid chromatographic/mass spectrometric separation was performed on a reverse phase column using a solvent system of methanol alone or methanol + 2-propanol. This method seemed promising for application to both qualitative and quantitative micro-analysis of fatty acids including very long chain fatty acids.
This article was published in J Biochem and referenced in Journal of Environmental & Analytical Toxicology

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