alexa Microwave-assisted cyclic amidine synthesis using TiCl4.
Chemistry

Chemistry

Organic Chemistry: Current Research

Author(s): Hellal M, Bihel F, Mongeot A, Bourguignon JJ

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Abstract Microwave-assisted treatment of various heterocyclic amides (benzodiazepinone, phthalazone) with TiCl(4) in the presence of primary or secondary amines provides the corresponding amidines. In addition to the interest of the microwaves for this reaction, our study highlights the higher reactivity of the cyclic acetamide moiety compared to the cyclic benzamide moiety towards this TiCl(4)-mediated reaction. This article was published in Org Biomol Chem and referenced in Organic Chemistry: Current Research

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