alexa Revisiting nucleophilic substitution reactions: microwave-assisted synthesis of azides, thiocyanates, and sulfones in an aqueous medium.
Biochemistry

Biochemistry

Biochemistry & Analytical Biochemistry

Author(s): Ju Y, Kumar D, Varma RS

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Abstract A practical, rapid, and efficient microwave (MW) promoted synthesis of various azides, thiocyanates, and sulfones is described in an aqueous medium. This general and expeditious MW-enhanced nucleophilic substitution approach uses easily accessible starting materials such as halides or tosylates in reaction with alkali azides, thiocyanates, or sulfinates in the absence of any phase-transfer catalyst, and a variety of reactive functional groups are tolerated. This article was published in J Org Chem and referenced in Biochemistry & Analytical Biochemistry

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