alexa Synthesis, mesomorphic and dielectric properties of 4-(cyanomethoxy)phenyl 4-alkoxybenzoates, 4-(cyanomethoxy)-4′-alkoxyazo- and -azoxybenzenes
Chemical Engineering

Chemical Engineering

Journal of Chromatography & Separation Techniques

Author(s): S A Kuvshinova, V A Burmistrov, I V Novikov, K M Litov, V V Aleksandriiskii

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Preparation methods were developed for homologs of 4-(cyanomethoxy)phenyl 4-alkoxybenzoates (C7, C8, C9), 4-(cyanomethoxy)-4′-alkoxyazo (C2, C3, C6), -azoxybenzenes (C3, C6) whose composition and structure were proved by elemental analysis and 1H NMR spectra. 4-(Cyanomethoxy) group destabilizes the mesophase, consequently, only four among the compounds obtained exhibit the thermotropic nematic mesomorphism. Original Russian Text © S.A. Kuvshinova, V.A. Burmistrov, I.V. Novikov, K.M. Litov, V.V. Aleksandriiskii, O.I. Koifman, 2014, published in Zhurnal Organicheskoi Khimii, 2014, Vol. 50, No. 5, pp. 631–636.

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This article was published in Russian Journal of Organic Chemistry and referenced in Journal of Chromatography & Separation Techniques

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