| |
|
Spiked TMHP concentration (ng/ml) |
Measured TMHP concentration (ng/ml) |
RSD (%) |
RE (%) |
| Within-run |
Day 1, n=5 |
1.990 |
1.894 |
3.8 |
-4.8 |
| 5.970 |
5.945 |
6.1 |
-0.4 |
| 99.50 |
91.46 |
3.7 |
-8.1 |
| 298.5 |
276.0 |
6.0 |
-7.6 |
| Day 2, n=5 |
1.990 |
2.238 |
4.4 |
12.4 |
| 5.970 |
6.168 |
3.8 |
3.3 |
| 99.50 |
91.36 |
1.9 |
-8.2 |
| 298.5 |
273.2 |
1.6 |
-8.5 |
| Day 3, n=5 |
1.990 |
2.040 |
9.5 |
2.5 |
| 5.970 |
6.089 |
6.2 |
2.0 |
| 99.50 |
95.78 |
3.5 |
-3.7 |
| 298.5 |
295.1 |
2.5 |
-1.1 |
| Between-run |
3 days, n=15 |
1.990 |
2.057 |
9.3 |
3.4 |
| 5.970 |
6.067 |
5.3 |
1.6 |
| 99.50 |
92.87 |
3.7 |
-6.7 |
| 298.5 |
281.4 |
5.0 |
-5.7 |
|
