| *Nominal Level |
*Measured Level of VD-2 |
*Measured Level of VD-3 |
| |
Mean |
SD |
CV (%) |
Bias (%) |
Mean |
SD |
CV (%) |
Bias (%) |
| Intra-run |
| 15 |
15.3 |
1.3 |
8.4 |
2.0 |
16.0 |
0.9 |
5.7 |
6.6 |
| 50 |
55.3 |
1.0 |
1.8 |
10.6 |
50.9 |
3.8 |
7.4 |
1.8 |
| 90 |
83.1 |
3.7 |
4.4 |
-7.6 |
97.3 |
1.1 |
1.4 |
8.1 |
| Inter-run |
| 15 |
14.8 |
1.2 |
8.2 |
-1.3 |
15.8 |
1.0 |
6.1 |
5.3 |
| 50 |
52.5 |
4.1 |
7.8 |
5.0 |
48.8 |
4.5 |
9.2 |
-2.4 |
| 90 |
86.0 |
5.6 |
6.5 |
-4.4 |
78.2 |
2.0 |
2.6 |
-13.1 |
| *Nominal Level |
*Measured Level of 25(OH)VD-2 |
*Measured Level of 25(OH)VD-3 |
| |
Mean |
SD |
CV (%) |
Bias (%) |
Mean |
SD |
CV (%) |
Bias (%) |
| Intra-run |
| 15 |
16.1 |
0.9 |
5.7 |
7.3 |
14.3 |
1.4 |
9.7 |
-4.6 |
| 50 |
50 |
2.1 |
3.9 |
7.8 |
54.9 |
2.7 |
4.8 |
9.7 |
| 90 |
97.4 |
6.1 |
6.2 |
8.2 |
97.3 |
4.4 |
4.5 |
8.4 |
| Inter-run |
| 15 |
16.4 |
0.7 |
4.0 |
9.3 |
14.7 |
1.3 |
8.6 |
-1.9 |
| 50 |
52.7 |
4.0 |
7.5 |
5.4 |
54.8 |
2.4 |
4.4 |
9.6 |
| 90 |
94.4 |
8.1 |
8.6 |
4.8 |
94.1 |
7.1 |
7.6 |
4.5 |
*nanogram/mL. SD, standard deviation, CV, standard deviation divided by mean measured concentration x 100. Bias, measured level - nominal level divided by nominal
level x 100. |
