| |
Previous Method |
Proposed Method |
| FLX |
N-FLX |
FLX |
N-FLX |
|
| Retention times |
7.7 |
3.4 |
4.24 |
2.49 |
| % Recovery (n = 6) |
86-88 |
92-93 |
98-102 |
98-102 |
| Tailing factor |
- |
- |
1.275 |
1.275 |
| Resolution |
Poorer |
Poorer |
6.625 |
8.161 |
| % Accuracy (n = 6) |
97-100 |
98-100 |
98-100 |
98-100 |
(%) C.V. inter-day
(n = 6) |
7.56 |
5.7 |
0.90 |
1.41 |
| (%)C.V. intra-assay (n = 6) |
2.66 |
2.16 |
0.97 |
1.02 |
|
