| |
2.5 ng/mL (LQC) |
20 ng/mL (LQC) |
250 ng/mL (MQC) |
750 ng/mL (HQC) |
| |
112.7 |
98.1 |
98.6 |
97.7 |
| |
105.8 |
97.4 |
98.3 |
97.6 |
| Day1 |
91.2 |
95.6 |
98.2 |
98.2 |
| |
89.1 |
93.2 |
98.9 |
98.9 |
| |
92.4 |
94.1 |
98.0 |
95.2 |
| |
90.1 |
94.8 |
100.0 |
98.6 |
| |
86.4 |
95.5 |
98.1 |
99.2 |
| intra-day 1
% intended value ± % CV |
95.4 ± 10.3 |
95.5 ± 1.8 |
98.6 ± 0.7 |
97.9 ± 1.4 |
| |
105.4 |
109.6 |
103.5 |
105.6 |
| |
94.6 |
106.3 |
104.4 |
99.8 |
| Day 2 |
103.2 |
110.9 |
102.4 |
96.4 |
| |
97.3 |
104.6 |
106.9 |
99.8 |
| |
94.6 |
107.8 |
103.8 |
104.2 |
| |
99.1 |
109.9 |
104.8 |
104.2 |
| |
97.6 |
110.5 |
100.2 |
96.3 |
| intra-day 2
% intended value ± % CV |
98.8 ± 4.2 |
108.5 ± 2.2 |
103.7 ± 2.0 |
100.9 ± 3.8 |
| |
88.3 |
104.4 |
97.9 |
102.3 |
| |
91.6 |
101.6 |
93.9 |
98.6 |
| Day3 |
107.5 |
105.3 |
105.2 |
104.5 |
| |
97.8 |
106.2 |
104.5 |
99.4 |
| |
104.8 |
107.4 |
101.9 |
101.4 |
| |
102.8 |
106.0 |
105.5 |
102.2 |
| |
110.8 |
107.3 |
108.5 |
101.6 |
| intra-day 3
% intended value ± % CV |
100.5 ± 8.3 |
105.5 ± 1.9 |
102.5 ± 4.9 |
101.4 ± 1.9 |
|
inter-day
% intended value ± % CV |
98.2 ±7.9 |
103.2 ± 5.8 |
101.6 ± 3.7 |
100.0 ± 2.9 |
|
