Sample |
Method |
Manifested
by |
Taken
mg mL−1 |
Added
mg mL−1 |
Found* |
Recovery
% |
S.D.
% |
Proposed |
Official |
Motilium
10 mg/tablet |
BCG |
Janssen
Pharmaceutical
N.V. ** |
3.0 |
|
2.98 |
2.97 |
99.33 |
0.83 |
|
|
3.0 |
6.02 |
5.96 |
100.33 |
0.52 |
|
|
6.0 |
9.05 |
8.95 |
100.56 |
0.78 |
|
|
9.0 |
12.10 |
12.07 |
100.83 |
1.12 |
|
MO |
|
4.0 |
|
>3.96 |
4.01 |
99.00 |
0.63 |
|
|
|
|
4.0 |
7.95 |
8.02 |
99.38 |
0.85 |
|
|
|
|
8.0 |
11.93 |
12.07 |
99.42 |
0.46 |
|
|
|
|
12.0 |
16.05 |
15.96 |
100.32 |
0.58 |
|
TCNE |
|
5.0 |
|
4.97 |
4.95 |
99.40 |
0.83 |
|
|
|
|
5.0 |
9.95 |
9.85 |
99.50 |
0.56 |
|
|
|
|
10.0 |
15.10 |
15.15 |
100.67 |
0.71 |
|
|
|
|
15.0 |
20.10 |
20.25 |
100.50 |
0.47 |
|
TCNQ |
|
6.0 |
|
5.97 |
5.96 |
99.50 |
0.94 |
|
|
|
|
6.0 |
12.05 |
12.07 |
100.42 |
1.11 |
|
|
|
|
12.0 |
18.10 |
18.20 |
100.56 |
0.83 |
|
|
|
|
15.0 |
20.90 |
21.25 |
99.52 |
0.79 |
|
|
|
|
|
|
|
|
|
Doxymycine
100 mg/
Capsule |
BCG |
Nile Co. ***
Pharmaceuticals
and Chemical Industries
N.V. |
3.0 |
|
2.95 |
2.98 |
98.33 |
0.63 |
|
|
3.0 |
5.92 |
6.03 |
98.67 |
0.51 |
|
|
6.0 |
8.96 |
9.04 |
99.56 |
0.88 |
|
|
9.0 |
12.07 |
12.11 |
100.58 |
1.03 |
|
MO |
4.0 |
|
3.98 |
3.98 |
99.50 |
0.41 |
|
|
|
|
4.0 |
8.07 |
7.96 |
100.88 |
0.57 |
|
|
|
|
8.0 |
11.98 |
11.95 |
99.83 |
0.81 |
|
|
|
|
12.0 |
16.15 |
16.05 |
100.94 |
0.47 |
|
TCNE |
|
5.0 |
|
5.02 |
4.96 |
100.40 |
0.92 |
|
|
|
|
5.0 |
10.03 |
9.92 |
100.30 |
1.05 |
|
|
|
|
10.0 |
14.96 |
15.10 |
99.73 |
0.88 |
|
|
|
|
15.0 |
19.93 |
20.15 |
99.65 |
0.96 |
|
TCNQ |
|
6.0 |
|
5.98 |
6.03 |
99.67 |
1.03 |
|
|
|
|
6.0 |
12.05 |
11.95 |
100.42 |
0.76 |
|
|
|
|
12.0 |
18.08 |
17.90 |
100.44 |
0.93 |
|
|
|
|
18.0 |
24.10 |
24.25 |
100.42 |
1.10 |
*Average of six determinations.
** Turnhoutseweg 30, B-2340 Beerse, Belgium.
*** Cairo, Egypt. |