| Storage condition |
Analyte concn.
(ng/mL) |
Calculated con.(ng/mL) |
% CV |
Accuracy (%) |
| Plasma |
Urine |
Plasma |
Urine |
Plasma |
Urine |
| Three freeze-thaw cycles |
100.80 |
105.96 ± 3.091 |
94.66 ± 4.737 |
2.9 |
5.0 |
105.1 |
93.9 |
| 8400.00 |
7902.81 ± 34.742 |
8059.43 ± 180.754 |
0.4 |
2.2 |
94.1 |
95.9 |
Autosampler
(24 hr) |
100.80 |
106.28 ± 4.775 |
107.68 ± 2.734 |
4.5 |
2.5 |
105.4 |
106.8 |
| 8400.00 |
7878.79 ± 168.324 |
7851.06 ± 285.283 |
2.1 |
3.6 |
93.8 |
93.5 |
Bench top
(6 hr) |
100.80 |
104.81 ± 2.272 |
100.65 ± 5.470 |
2.2 |
5.4 |
104.0 |
99.9 |
| 8400.00 |
8037.10 ± 133.286 |
8057.51 ± 259.936 |
1.7 |
3.2 |
95.7 |
95.9 |
|
